Anhydrous reaction method for preparing polymeric ferric sulfate
A technology for polymerizing ferric sulfate and water reaction, applied in the direction of ferric sulfate, chemical recovery, etc., can solve the problems of long reaction time, large amount of catalyst, many equipment, etc., and achieve the effect of reducing production cost, energy consumption, and waste gas.
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[0009] Anhydrous reaction produces the method for polyferric sulfate, and its step is:
[0010] 1. In a professional stainless steel reaction device with a volume of 2-20 cubic meters, add 2-20 tons of industrial ferrous sulfate and 0.2-1.8 tons of sulfuric acid successively; industrial ferrous sulfate: sulfuric acid is 10:1;
[0011] 2. In a near-vacuum state, put 2.5-3.5kg of catalyst into the stainless steel reaction device per ton of ferrous sulfate, and use sodium nitrite or dilute nitric acid as the catalyst;
[0012] 3. Open the oxygen valve of the reaction device, and when it reaches 0.02MPa, turn on the pump stirring, maintain the pressure at 0.02-0.04MPa, and keep the reaction temperature within 100°C until the oxygen pressure remains unchanged; after 3-10 hours, the sampling analysis is qualified , open the vent valve, a small amount of tail gas is sent to the alkali absorption tower for treatment, and after the alkali solution is saturated, it can be returned to be...
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