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Heavy oil separation method and treatment system thereof

A separation method and technology of a treatment system, applied in the field of heavy oil separation method and its treatment system, can solve the problems of insignificant separation effect of heavy oil raw materials, etc., achieve the solution of insignificant separation effect, high yield, and improve separation effect Effect

Active Publication Date: 2016-03-16
CHINA UNIV OF PETROLEUM (BEIJING)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The main technical problem to be solved by the present invention is to provide a heavy oil separation method and its processing system, which can effectively solve the problem of insignificant separation effect of heavy oil raw materials in the extraction and separation process in the prior art, thereby Obtain the target product with high yield and excellent properties

Method used

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  • Heavy oil separation method and treatment system thereof
  • Heavy oil separation method and treatment system thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0062] Use petroleum residue (boiling point> 420°C) as the raw material, using a C3-C4 mixed solvent (wherein, the main solvent, the auxiliary solvent and the supercritical solvent are all the mixed solvents), the composition of the mixed solvent is as follows:

[0063] Component Propane Isobutane N-butane Composition, m%255025

[0064] Such as figure 2 As shown, the three-stage separation method is used to separate petroleum residue. For the specific process, please refer to the above-mentioned three-stage separation method. The process parameters involved in each step of the method are as follows:

[0065] 1) The mass flow rate ratio of main solvent and petroleum residue is 2.4:1;

[0066] 2) The mass flow rate ratio of secondary solvent and petroleum residue is 0.1:1;

[0067] 3) The mixing temperature of petroleum residue and main solvent is 120℃, and the pressure is 4.6MPa;

[0068] 4) Three-stage packing is installed in the upper area of ​​the extraction tower 02, the packi...

Embodiment 2

[0077] Use petroleum residue (boiling point> 420°C) as the raw material, using a C4 mixed solvent (wherein, the main solvent, the secondary solvent and the supercritical solvent are all the mixed solvent), and the composition of the mixed solvent is as follows:

[0078] Component Isobutane N-butane Composition, m%2575

[0079] Such as figure 2 As shown, the three-stage separation method is used to separate petroleum residue. For the specific process, please refer to the above-mentioned three-stage separation method. The process parameters involved in each step of the method are as follows:

[0080] 1) The mass flow rate ratio of main solvent and petroleum residue is 2.8:1;

[0081] 2) The mass flow rate ratio of secondary solvent to petroleum residue is 0.2:1;

[0082] 3) The mixing temperature of petroleum residue and main solvent is 100℃, and the pressure is 4.3MPa;

[0083] 4) The upper area of ​​the extraction tower 02 is filled with 4 sections of packing, the packing is rand...

Embodiment 3

[0093] The bottom product (atmospheric residual oil) obtained by atmospheric distillation of Canadian oil sands pitch (boiling point> 350℃, density at 20℃> 1.0g / cm 3 ) Is the raw material, using a C5 mixed solvent (wherein, the main solvent, the auxiliary solvent and the supercritical solvent are all the mixed solvent), and the composition of the mixed solvent is as follows:

[0094] Component Isopentane N-pentane Composition, m%2575

[0095] Such as figure 2 As shown, the three-stage separation method is used to separate the atmospheric residue. For the specific process, please refer to the above-mentioned three-stage separation method. The process parameters involved in each step of the method are as follows:

[0096] 1) The mass flow rate ratio of main solvent to atmospheric residue is 2.75:1;

[0097] 2) The mass flow rate ratio of secondary solvent to atmospheric residue is 0.25:1;

[0098] 3) The mixing temperature of atmospheric residue and main solvent is 170℃, and the p...

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Abstract

The present invention provides a heavy oil separation method and a treatment system thereof. According to the separation method, an extraction tower with a plurality of filler sections arranged on the upper portion region is used, distributors are arranged between the adjacent filler sections, and a supercritical solvent from a supercritical solvent recovery tower is introduced through the distributors so as to further separate the heavy components in the deasphalted oil phase on the upper portion of the extraction tower. With the separation method of the present invention, the problem that the heavy oil raw material separation effect is not significant during the extraction separation process in the prior art can be effectively solved so as to obtain the target product with characteristics of high yield and excellent property.

Description

Technical field [0001] The invention relates to a method for separating heavy oil and a processing system thereof, and belongs to the technical field of petroleum processing. Background technique [0002] Solvent deasphalting is a technology that removes the heavy component bitumen from heavy petroleum oil. It is suitable for heavy oil, oil sand bitumen and various atmospheric and vacuum residues obtained during petroleum processing. Treatment, the density of this type of heavy oil (20℃)> 0.934g / cm 3 Or the boiling point is higher than 350°C. The deasphalted oil is mainly used to produce lubricating oil base oil or as a raw material for subsequent processing of catalytic cracking or hydrocracking (not limited to), and the removed asphalt can be used as road asphalt, construction asphalt or gasification raw material. [0003] The existing solvent deasphalting technology mainly has two or three stages. In the secondary extraction and separation process, in the first stage, the s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10G53/00
Inventor 赵锁奇许志明孙学文徐春明
Owner CHINA UNIV OF PETROLEUM (BEIJING)