Preparation method for high-strength pure titanium panels

A high-strength, pure titanium technology, applied in the field of metal materials, can solve the problems of difficulty in preparing large-volume materials, severe plastic deformation, and small size of deformed pure titanium, achieving high local shear sensitivity and less slip system. , the effect of increasing strength

Active Publication Date: 2016-04-13
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] However, for pure titanium with hexagonal close-packed metal, there are problems such as difficulty in severe plastic deformation and deformation cracking at room temperature due to the small number of slip systems.
At present, the severe plastic deformation method used for pure titanium mainly includes High Pressure Torsion (HPT), but the deformed pure titanium obtained by HPT method is very small in size, and it is difficult to prepare large-volume materials; ARB) has strict requirements on the superimposed surface of the plate, the roll surface and the ambient atmosphere. This method is limited to the preparation of pure titanium composite thin strips, and the material composite interface is easy to cause cracks.
Equal channel angular pressing (ECAP) is a large plastic deformation process newly developed in recent years to refine the grain and improve the strength of the material. However, the ECAP deformation of pure titanium is usually carried out at medium temperature, and it is still only applicable For the production of small-sized rods, there are still certain limitations for the preparation of large-sized pure titanium plates, and the consumption of molds is serious

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  • Preparation method for high-strength pure titanium panels
  • Preparation method for high-strength pure titanium panels
  • Preparation method for high-strength pure titanium panels

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The method for preparing a high-strength pure titanium plate by using the pure titanium plate TA1 with a size of 78×78×2mm as a raw material is carried out according to the following process steps:

[0026] (1) Use a controllable pressure testing machine to limit the severe plastic deformation of the pure titanium plate TA1 at room temperature. The process parameters are: the tooth width of the bending die of the molding die is 2mm, the tooth height is 2mm, and the deformation rate is 10~20mm / min , 3-pass deformation;

[0027] (2) Perform electric pulse annealing treatment on the pure titanium plate between each pass to limit the molding deformation, that is, electric pulse annealing treatment. The process parameters are: pulse current density is 0.3~0.6kA / mm 2 , the pulse current frequency is 20~30Hz, the pulse width is 30μs, the processing time is 2~10min, and the number of electric pulse annealing treatments is 2 times;

[0028] (3) A high-strength pure titanium pla...

Embodiment 2

[0031] The method for preparing a high-strength pure titanium plate using the pure titanium plate TA1ELI with a size of 102×102×1.5mm as a raw material is carried out according to the following process steps:

[0032] (1) Use a controllable pressure testing machine to limit the severe plastic deformation of the pure titanium plate TA1ELI at room temperature. The process parameters are: the tooth width of the bending die of the molding die is 1.5mm, the tooth height is 1.5mm, and the deformation rate is 3~10mm / min, 2-pass deformation;

[0033] (2) Perform electric pulse annealing treatment on the pure titanium plate between each pass to limit the molding deformation, that is, electric pulse annealing treatment. The process parameters are: pulse current density is 0.2~0.4kA / mm 2 , the pulse current frequency is 10~30Hz, the pulse width is 10μs, the processing time is 1~5min, and the frequency of electric pulse annealing treatment is 1 time;

[0034] (3) A high-strength pure ti...

Embodiment 3

[0037] The method for preparing a high-strength pure titanium plate with a size of 52×52×3mm pure titanium plate TA2 as a raw material is carried out according to the following process steps:

[0038] (1) Use a controllable pressure testing machine to limit the severe plastic deformation of the pure titanium plate TA2 at room temperature. The process parameters are: the tooth width of the bending die of the molding die is 3mm, the tooth height is 3mm, and the deformation rate is 30~40mm / min , 3-pass deformation;

[0039] (2) Perform electric pulse annealing treatment on the pure titanium plate between each pass to limit the molding deformation, that is, electric pulse annealing treatment. The process parameters are: pulse current density is 0.5~0.8kA / mm 2 , the pulse current frequency is 20~40Hz, the pulse width is 20μs, the processing time is 5~15min, and the number of electric pulse annealing treatments is 2 times;

[0040] (3) A high-strength pure titanium plate is obtaine...

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Abstract

The invention provides a preparation method for high-strength pure titanium panels. The preparation method comprises the technological steps that 1, a pure titanium panel is subjected to constrained groove pressing severe plastic deformation at the room temperature by adopting a pressure-controllable testing machine; 2, the pure titanium panel is subjected to electric pulse annealing treatment during every pass of constrained groove pressing deformation; and 3, the high-strength pure titanium panel is obtained after treatment at the last pass of constrained groove pressing severe plastic deformation. According to the preparation method, the advantages of severe plastic deformation and electric pulse treatment are integrated, so that the problems that hard-deformation hexagonal closed-packed metal pure titanium can be hardly subjected to room-temperature severe plastic deformation, and cracking occurs during a deformation process are solved; the large-sized high-strength pure titanium panel can be prepared; and compared with the original pure titanium panel, the increasing rate of yield strength of the large-sized high-strength pure titanium panel exceeds 160% at most, and the increasing rate of extension strength exceeds 80% at most.

Description

technical field [0001] The invention relates to a preparation method in the technical field of metal materials, in particular to a preparation method of high-strength pure titanium plate. Background technique [0002] With its low density, high specific strength and specific stiffness, good corrosion resistance, especially good high temperature durability and excellent biocompatibility, pure titanium is widely used in biomedicine, aerospace, automobile, biology, etc. field has been widely used. However, although pure titanium has good plasticity, its low strength as a bearing part, poor wear resistance, and difficulty in deformation at room temperature restrict the development and application of pure titanium. [0003] Grain refinement is an important way to improve material strength and comprehensive mechanical properties, and it is also the only method that can simultaneously increase material strength and improve material toughness. At present, there are many methods an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22F3/00C22F1/18
CPCC22F1/183C22F3/00
Inventor 王磊宋秀刘杨
Owner NORTHEASTERN UNIV
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