Modified graphene doped lithium cobaltate battery cathode material and preparation method thereof
A cathode material, graphene technology, applied in battery electrodes, circuits, electrical components, etc., can solve problems such as restricting development prospects, lack of cobalt resources, toxicity, etc., to prolong storage time, improve self-discharge, and simple methods.
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[0010] The modified graphene-doped lithium cobaltate battery positive electrode material is prepared by the following components according to the ratio shown in parts by weight, graphene oxide 55, lithium manganate 65, 45% lithium iron nitrate solution 25, scale Graphite 3, bonding material 3.
[0011] The preparation method of the modified graphene-doped lithium cobalt oxide cathode material comprises the following steps:
[0012] (1) Get graphite and sodium nitrate, place in a certain amount of concentrated sulfuric acid in an ice bath with a mass ratio of 2:1, add potassium percobaltate 3 times the quality of the graphite under stirring, mix evenly, and control the temperature to low Stir at 20°C for about 1h, then increase the temperature to 32-38°C for 2h, slowly add quantitative deionized water dropwise, stir well, add hydrogen peroxide to terminate the reaction when the system temperature drops, filter, wash, dry; heat and stir In the process of adding a certain amount...
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