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A reinforcement and protection agent for crisp powder murals and its preparation and reinforcement method

A technology for reinforcement and murals, applied in the preservation of paintings, decorative arts, etc., can solve the problems of material aging, poor penetration of reinforcement reagents, and fouling of the paint layer on the surface of murals, and achieve the reduction of water holding and hygroscopicity, and the inhibition of salt damage. The effect is obvious and the water volatility is improved

Active Publication Date: 2017-03-22
SHAANXI NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, after the test of timeliness, the organic protective reagent has passed the test of the environment, and there have been phenomena such as material aging, which has caused certain protective damage to the mural itself.
Inorganic reagents have good aging resistance, but some reinforcement reagents have poor permeability, do not form concentration gradients and strength gradients, and are easy to form hard shells on the reinforcement layer on the surface of murals, causing the reinforcement layer on the surface of murals to fall off, and some reinforcement reagents are also likely to cause surface whitening. Some damage to the paint layer on the surface of the mural

Method used

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  • A reinforcement and protection agent for crisp powder murals and its preparation and reinforcement method
  • A reinforcement and protection agent for crisp powder murals and its preparation and reinforcement method
  • A reinforcement and protection agent for crisp powder murals and its preparation and reinforcement method

Examples

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Embodiment 1

[0033] A kind of crisp powder mural protection reinforcing agent, described crisp powder mural reinforcing material includes TB-1, TB-2, TB-3 and TB-4 reinforcing agent, wherein, TB-1 reinforcing agent is every 1000 milliliters of ethanol Dissolve 150ml of tetraethyl orthosilicate in a colorless and clear solution, TB-2 reinforcement is a colorless and clear solution of 2 grams of oxalic acid and 2 milliliters of phosphoric acid dissolved in every 1000 milliliters of ethanol, TB-3 reinforcement is a colorless and clear solution in every 1000 milliliters of ethanol A colorless and clear solution of 5 grams of barium hydroxide of 100-200 nanometer level developed by a ball mill dissolved in milliliters of methanol, and the TB-4 reinforcing agent is a colorless and clear solution of 3 grams of sodium octaborate dissolved in 100 milliliters of water; The chemical raw materials mentioned above are industrial pure. Among them, the appropriate volume ratio of the four reagents TB1, T...

Embodiment 2

[0046] A kind of crisp powder mural protection reinforcing agent, described crisp powder mural reinforcing material includes TB-1, TB-2, TB-3 and TB-4 reinforcing agent, wherein, TB-1 reinforcing agent is every 1000 milliliters of ethanol Dissolve 250ml of tetraethyl orthosilicate in a colorless and clear solution, TB-2 reinforcement is a colorless and clear solution in which 5 grams of oxalic acid and 5 milliliters of phosphoric acid are dissolved in every 1000 milliliters of ethanol, and TB-3 reinforcement is a colorless and clear solution in every 1000 milliliters of ethanol A colorless and clear solution of 10 grams of barium hydroxide and 3 grams of polyethylene glycol (200 molecular weight) developed by a ball mill and 3 grams of polyethylene glycol (200 molecular weight) dissolved in milliliters of methanol, 5 grams of TB-4 reinforcement is dissolved in 100 milliliters of water A colorless clear solution of sodium octaborate; the chemical raw materials are all technicall...

Embodiment 3

[0059] A kind of crisp powder mural protection reinforcing agent, described crisp powder mural reinforcing material includes TB-1, TB-2, TB-3 and TB-4 reinforcing agent, wherein, TB-1 reinforcing agent is every 1000 milliliters of ethanol Dissolve 200ml of tetraethyl orthosilicate in a colorless and clear solution, TB-2 reinforcement is a colorless and clear solution in which 3 grams of oxalic acid and 3 milliliters of phosphoric acid are dissolved in every 1000 milliliters of ethanol, and TB-3 reinforcement is a colorless and clear solution in every 1000 milliliters of ethanol A colorless and clear solution of 7 grams of barium hydroxide and 2.5 grams of polyethylene glycol (200 molecular weight) developed by a ball mill and 2.5 grams of polyethylene glycol (200 molecular weight) dissolved in milliliters of methanol, TB-4 reinforcement is dissolved in 100 milliliters of water 4 grams A colorless clear solution of sodium octaborate; the chemical raw materials are all technicall...

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Abstract

The invention provides a flaked and powdered mural reinforcing protective agent and a preparation and reinforcing method thereof. The agent is prepared from a reinforcing agent TB-1 prepared by dissolving 150-250 ml of ethyl orthosilicate in 1000 ml of ethyl alcohol, a reinforcing agent TB-2 prepared by dissolving 2-5 g of oxalic acid and 2-5 ml of phosphoric acid in each 1000 ml of ethyl alcohol, a reinforcing agent TB-3 prepared by 5-10 g of barium hydroxide and 2-3 g of poly(ethylene glycol) which are ground into the 100-200 nanometer scale through a ball mill in each 1000 ml of methyl alcohol, and a reinforcing agent TB-4 prepared by dissolving 3-5 g of disodium octoborate tetrahydrate in 100 ml of water according to the volume ratio of (2-5):(7-10):(7-10):(0.5-1.5). The coffin chamber flaked and powdered mural reinforcing material and the reinforcing method which are suitable for dry, semi-dry and humid environment conditions of arid regions, semi-arid regions and semi-humid regions are obtained.

Description

technical field [0001] The invention relates to the technical field of cultural relics protection, in particular to a reinforcement and protection agent for crispy powder murals and a preparation and reinforcement method thereof. Background technique [0002] As an important part of traditional Chinese murals, tomb murals are generally painted on the four walls, the top and both sides of the corridor of the tomb. Most of the murals in the tomb reflect the activities of the deceased during his lifetime, and there are also gods, myths and legends, historical stories, sun, moon, stars, and pattern decorations. Considering the principles of authenticity and integrity of cultural heritage, and because some tomb murals are difficult to remove due to the special drawing process, many important tomb murals are protected in situ. [0003] The tomb murals are affected by the environment such as changes in temperature and humidity, harmful gases in the air, and light intensity. After ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B44D7/00C08L71/08C08K3/22
CPCB44D7/00C08K3/22C08L71/00
Inventor 李玉虎戎岩傅鹏
Owner SHAANXI NORMAL UNIV
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