Method for preparing aluminum-free magnesium-based composite materials by aid of Al-Ti-X self-propagating systems
A composite material, al-ti-x technology, used in the preparation of aluminum-free magnesium-based composite materials using an Al-Ti-X self-propagating system, and the preparation of magnesium-based composite materials. The spread system cannot be applied to aluminum-free magnesium alloys, etc., to achieve the effect of simple process, easy popularization and application, and low production cost
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Embodiment 1
[0017] Step 1, using magnesium ingots and zinc ingots to smelt Mg-6Zn magnesium-based melts;
[0018] Step 2: Select the Al-Ti-B self-propagating system, ignite the self-propagating reaction in the vacuum heating device, and synthesize TiB in situ 2 Reinforce the particles, and then add the reacted Al-Ti-B prefabricated block into the magnesium liquid to prepare a Mg-6Zn magnesium-based composite material melt; the mass ratio of the added self-propagating prefabricated block to the magnesium-based melt is 10 : 100;
[0019] Step 3, adding Y element to the magnesium-based composite material melt and stirring, so that it consumes the residual Al element after the reaction of the Al-Ti-B system to obtain a composite material melt; the atomic ratio of the Y element to the residual Al element is 1 :2.
[0020] Step 4, adding the Zr element into the melt of the composite material, and fully stirring. After heat preservation and standing, cast and form to obtain in-situ TiB 2 Par...
Embodiment 2
[0022] Step 1, using magnesium ingots and zinc ingots to smelt Mg-8Zn magnesium-based melts;
[0023] Step 2: Select the Al-Ti-C self-propagating system, add the Al-Ti-C prefabricated block directly into the magnesium liquid, use the magnesium liquid to ignite the self-propagating reaction at high temperature, and synthesize TiC reinforced particles in situ, thus obtaining Mg- 8Zn magnesium-based composite material melt; the mass ratio of the added self-propagating prefabricated block to the magnesium-based melt is 4:100;
[0024] Step 3, adding element Y to the melt of the magnesium-based composite material and stirring to consume the residual Al element after the reaction of the Al-Ti-C system. The atomic ratio of the added amount of Y element to the residual Al element is 1.1:2.
[0025] Step 4, adding the Zr element into the melt of the composite material, and fully stirring. After standing still for heat preservation, it was poured and molded to obtain in-situ TiC parti...
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