Natural mango dye based on mango yellow pigment and preparation method of natural mango dye

A yellow pigment and mango technology, applied in natural dyes, dyeing methods, azo dyes, etc., can solve the problems of low comprehensive utilization rate, environmental hazards, and few applications, and achieve good biodegradability and environmental compatibility. The effect of high dye uptake and high dye content

Inactive Publication Date: 2016-06-29
SUZHOU INSILK CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, natural pigments are widely used in the food industry as food pigments, and are less used in other aspects, and the comprehensive utilization rate is not high.
[0005] my country is a big textile country, and dyeing and finishing is an indispensable link in textiles. However, most of the dyes currently used are synthetic dyes, which are extremely harmful to the environment.

Method used

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  • Natural mango dye based on mango yellow pigment and preparation method of natural mango dye

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] (1) Clean the fresh and ripe mango, remove the pulp, boil the mango skin in boiling water for 30 seconds to remove the activity of the enzyme, take it out, dry it, and chop it to obtain a volume less than 5mm 3 of crushed mango peel.

[0028] (2) In parts by weight, immerse the pulverized mango peel obtained in 10 parts of step (1) in 100 parts of 80% ethanol aqueous solution, and extract repeatedly 3 times until the extract is colorless, and the extracts are combined and mixed , after 500W ultrasonic treatment for 5min and ultrafiltration membrane filtration, concentrated to obtain a filtrate with a mango yellow pigment content of 49%.

[0029] (3) in parts by weight, add 20 parts of hydrolyzed chitosan, 25 parts of aloe gel and 10 parts of deionized water in the filtrate containing mango yellow pigment prepared by 35 parts of step (2), Stir at 35° C. for 30 minutes at a speed of 500 rpm / min to obtain a natural mango dye based on mango yellow.

Embodiment 2

[0031] (1) Clean the fresh and ripe mango, remove the pulp, boil the mango skin in boiling water for 30 seconds to remove the activity of the enzyme, take it out, dry it, and chop it to obtain a volume less than 5mm 3 of crushed mango peel.

[0032] (2) In parts by weight, immerse the pulverized mango peel obtained in 10 parts of step (1) in 100 parts of 100% ethanol aqueous solution, and extract repeatedly 4 times until the extract is colorless, and the extracts are combined and mixed , after 800W ultrasonic treatment for 10min and ultrafiltration membrane filtration, concentrated to obtain a filtrate with a mango yellow pigment content of 61%.

[0033] (3) by weight, add 30 parts of hydrolyzed chitosan, 30 parts of aloe gel and 30 parts of deionized water in the filtrate containing mango yellow pigment prepared by 50 parts of step (2), Stir at 800 rpm / min for 50 min at 45° C. to obtain a natural mango dye based on mango yellow.

Embodiment 3

[0035] (1) Clean the fresh and ripe mango, remove the pulp, boil the mango skin in boiling water for 30 seconds to remove the activity of the enzyme, take it out, dry it, and chop it to obtain a volume less than 5mm 3 of crushed mango peel.

[0036] (2) In parts by weight, immerse the pulverized mango peel obtained in 10 parts of step (1) in 100 parts of 90% ethanol aqueous solution, and extract repeatedly 3 times until the extract is colorless, and the extracts are combined and mixed , after 600W ultrasonic treatment for 8min and ultrafiltration membrane filtration, concentrated to obtain a filtrate with a mango yellow pigment content of 52%.

[0037] (3) by weight, add 28 parts of hydrolyzed chitosan, 27 parts of aloe gel and 15 parts of deionized water in the filtrate containing mango yellow pigment prepared by 40 parts of steps (2), Stir at 40° C. for 40 minutes at a speed of 700 rpm / min to obtain a natural mango dye based on mango yellow pigment.

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Abstract

The invention provides a natural mango dye based on mango yellow pigment and a preparation method thereof. The specific operation steps are: (1) clean the fresh and ripe mango, remove the pulp, boil the mango peel in boiling water for 30 seconds to remove the activity of the enzyme , take out and dry, chop to obtain crushed mango peel; (2) immerse the crushed mango peel in a solvent, and extract repeatedly 3-4 times until the extract is colorless, combine and mix the extract, and undergo ultrasonic treatment and After being filtered by an ultrafiltration membrane, it is concentrated to obtain a filtrate containing mango yellow pigment; (3) adding chitosan, aloe vera gel and deionized water to the filtrate containing mango yellow pigment, heating and stirring evenly to obtain a product. The natural mango dye based on mango yellow pigment prepared by the invention is non-toxic, non-polluting, green and degradable, has antibacterial, anti-ultraviolet and other health care effects, and is different from traditional fabric dyes in that it has high dye content and high dye extraction rate , The performance of the dye is stable, the dyeing rate of the dyed fabric is high, and the color fastness is good.

Description

Technical field: [0001] The invention belongs to the technical field of textile materials, and in particular relates to a natural mango dye based on mango yellow pigment and a preparation method thereof. Background technique: [0002] Mango, also known as An Luo Guo, Lime Fruit, Miwangzi, Xianggai, is rich in vitamins and sugars. It is a famous tropical fruit and is known as the king of tropical fruits. In recent years, my country's mango industry has also achieved rapid development. Development, the products prepared from mango mainly include mango jam, mango preserved, mango drink and so on. In the manufacturing process of mango products, a large amount of leftover mango skin, mango core and mango leaves will be produced. At present, the leftovers of mango production have not been fully utilized, which not only utilizes resources, but also pollutes the environment. [0003] At present, there have been many reports that pigments can be extracted from natural plants as raw m...

Claims

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Application Information

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IPC IPC(8): C09B61/00D06P1/34D06P1/48D06P1/44
CPCC09B61/00D06P1/34D06P1/44D06P1/48
Inventor 周继东
Owner SUZHOU INSILK CO LTD
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