Composite particles for electrodes of electrochemical devices
A technology for electrochemical components and composite particles, which is applied in the direction of electrical components, battery electrodes, hybrid capacitor electrodes, etc., can solve the problem that composite particles are not recorded, and achieve the effect of excellent flexibility and sufficient adhesion
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Embodiment 1
[0179] (Manufacture of particulate binder resin (B))
[0180] Add 47 parts of styrene, 50 parts of 1,3-butadiene, 3 parts of methacrylic acid, 4 parts of sodium dodecylbenzenesulfonate, and 150 parts of ion-exchanged water into a 5MPa pressure-resistant container with a stirrer, as After sufficiently stirring 0.4 parts of t-dodecylmercaptan as a chain transfer agent and 0.5 parts of potassium persulfate as a polymerization initiator, they were heated to 50° C. to initiate polymerization. Cooling was performed when the polymerization conversion ratio reached 96% to terminate the reaction to obtain a particulate binder resin (B) (styrene-butadiene copolymer; hereinafter also abbreviated as "SBR").
[0181] (Manufacture of slurry for composite particles)
[0182] As the negative electrode active material (A), 91.0 parts of artificial graphite (average particle diameter: 24.5 μm, graphite layer spacing (interplanar spacing (d value) of (002) plane measured by X-ray diffraction me...
Embodiment 2
[0194] Except that 97.6 parts of artificial graphite was used as the negative electrode active material (A), the manufacture of the slurry for composite particles, the manufacture of composite particles, the manufacture of negative electrodes for lithium ion secondary batteries, and the manufacture of lithium ion secondary batteries were carried out in the same manner as in Example 1. Manufacture of ion secondary batteries.
Embodiment 3
[0196] In addition to using a 1.0% aqueous dispersion of cellulose nanofibers as the water-insoluble polysaccharide polymer fiber (D) (raw material: conifer, degree of fibrillation: high, average degree of polymerization 300; manufactured by Chuetsu Pulp Co.), and Production of the slurry for composite particles, production of composite particles, production of negative electrodes for lithium ion secondary batteries, and production of lithium ion secondary batteries were performed in the same manner as in Example 1.
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