Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco

A technology for red dates and roasted sweetness is applied in the field of preparation of roasted sweet aroma components of red dates. Production application, increased sweetness, prominent effect of roasted sweetness

Active Publication Date: 2016-08-10
ZHENGZHOU TOBACCO RES INST OF CNTC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, domestic spice manufacturers mostly use the traditional low-alcohol ethanol continuous extraction method to prepare jujube extract. This method has two major disadvantages: ① part of the natural jujube aroma is lost during the extraction process, and the aroma of the product is weak; ② except for the aroma components in the product , the main components are sugar, pectin and protein substances, so that the application of the product is subject to certain restrictions
However, the resulting product still contains more protein, hemicellulose, pectin, pigments and other substances, which will be cracked to produce some harmful components during the smoking process of pipe tobacco, and at the same time increase the

Method used

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  • Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco
  • Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco
  • Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco

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Experimental program
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Effect test

Embodiment 1

[0028] ⑴ Preparation of Roasted Sweet Fragrance of Red Dates

[0029]Commercially available Xinjiang jujube (dried jujube), about 1.5 kg after being washed, pitted and sun-dried. Use 75% ethanol to heat to 60°C for extraction, the mass ratio of solid to liquid is 1:6, and extract twice for 2 hours each time. The two extracts were combined, first filtered with a 200 nm microfiltration membrane to collect the permeate, and then passed through a 5 kD ultrafiltration membrane to collect the ultrafiltration permeate. Concentrate the ultrafiltration permeate under reduced pressure to obtain 550 g without alcohol smell; at this time, add 300 g of distilled water, stir and mix well, and then put it on a D-101 macroporous adsorption resin chromatography column (the inner diameter of the column is 8 cm, and the packing height is 70 cm, with a column volume of about 3.5 L; the resin filler was purchased from Sinopharm Chemical Reagent Co., Ltd.), after standing for 6 h for adsorption, r...

Embodiment 2

[0048] Commercially available Xinzheng jujube (dried jujube) was washed, pitted, and dried at low temperature. Weighed 1 kg and extracted it with 65% ethanol in a circular ultrasonic cycle. The mass ratio of solid to liquid was 1:15. The extraction temperature was 35°C and the ultrasonic frequency was 40 kHz. The power was 750 W, the stirring speed was 1500 rpm, the extraction time was 50 min in total, and the ultrasonic time and interval time were 2 s / 1 s. The extract was filtered through a 50 nm microfiltration membrane, and then passed through a 5 kD ultrafiltration membrane to collect the ultrafiltration permeate. Concentrate the ultrafiltration permeate under reduced pressure until it has no alcohol smell to obtain 350 g of extract, add 200 g of deionized water, stir and mix well, and then put it on the AB-8 macroporous adsorption resin chromatography column (column inner diameter 6 cm, packing The height of the column is 60 cm, and the column volume is about 1.7 L; the r...

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Abstract

The invention belongs to the technical field of tobacco spice, and particularly relates to a method for preparing roasted fragrant and sweet components of red dates. The method comprises the steps that a, the red dates are washed, decored and dried; b, ethanol extraction is carried out; c, membrane separation is carried out to remove macromolecular matter; d, the materials pass through a macroporous adsorption resin chromatographic column to separate and acquire effective ingredients. The roasted fragrant and sweet components of the red dates contain rich monosaccharide, disaccharide and multiple roasted fragrance and sweet ingredients (furan, furanone, pyrone, cyclopentenone and other compounds), after the roasted fragrant and sweet components of the red dates are applied to the cut pipe tobacco, joyful roasted fragrant and sweet smells can be given to the pipe tobacco, the remaining taste is sweet and comfortable, and the pipe tobacco meets the favor of tobacco product consumers in China better. According to the preparation process of the roasted fragrant and sweet components of the red dates, ingredients having side effects on smoking of the pipe tobacco in red date crude extract can be effectively removed, two kinds of effective ingredients are separated and enriched, and the optimal application effect is achieved through effective blending of flavorists. The preparation process is simple and easy to operate, the production process is economical and environmentally friendly, and the method is suitable for being applied to large-scale industrial production.

Description

technical field [0001] The invention belongs to the technical field of spices for tobacco, in particular to a preparation method of roasted sweet aroma components of red dates and its application in pipe tobacco. The application of this technology does not change the existing processing technology of shredded pipe tobacco, and can increase the roasted-sweet aroma of shredded pipe tobacco when burning and smoking, increase sweetness and reduce irritation. Background technique [0002] Pipe tobacco is a tobacco product intended for smoking with a pipe. The main raw materials of pipe tobacco are sun-cured or air-cured and flue-cured tobacco, and mixed with appropriate amount of spices or vegetable oil. In recent years, the sales of cut pipe tobacco in foreign tobacco markets have continued to grow. Among them, from 2008 to 2011, the sales of cut pipe tobacco in the United States jumped from 3.5 million pounds to 30 million pounds (1 pound is about 0.45 kilograms). In 2013, S...

Claims

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Application Information

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IPC IPC(8): A24B3/12C11B9/02
CPCA24B3/12C11B9/025
Inventor 张文娟屈展洪广峰洪群业霍现宽张启东柴国璧姬凌波杨伟平徐秀娟何保江胡军
Owner ZHENGZHOU TOBACCO RES INST OF CNTC
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