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Preparation method of asphalt mixture sample ultrathin slice for microscopic observation

A technology of asphalt mixture and material flakes, which is applied in the preparation of test samples, analysis materials, sampling, etc., can solve the problems of inability to prepare complete and microcrack-free asphalt mixture ultrathin slices, and achieve resource saving and reduction. Low maintenance cost and extended service life

Inactive Publication Date: 2016-08-10
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The asphalt mixture specimen itself has a porous structure, and the objective existence of factors such as hard aggregates inside the mixture makes it possible to obtain only slices with a certain thickness (such as 10mm) by using traditional cutting and grinding methods, and cannot prepare Ultra-thin slices of asphalt mixture that are complete and without microcracks

Method used

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  • Preparation method of asphalt mixture sample ultrathin slice for microscopic observation
  • Preparation method of asphalt mixture sample ultrathin slice for microscopic observation
  • Preparation method of asphalt mixture sample ultrathin slice for microscopic observation

Examples

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Embodiment 1

[0031] In this example, the porous asphalt mixture sample has a porosity of 16.2%. The preparation method of the asphalt mixture super flakes includes the following steps:

[0032] 1) Cut the asphalt mixture into samples of asphalt mixture no more than 30mm×40mm×20mm (width×length×thickness), then immerse it in the uncured polyester material, and put 25 The epoxy resin with a viscosity of 2500mPa.s at ℃ is filled into the voids of the asphalt mixture sample, and the asphalt mixture sample filled with polyester material is obtained;

[0033] 2) The low-viscosity epoxy resin in the asphalt mixture sample to be filled with polyester material is cured for 48 hours, then cut into slices with a thickness of 4mm, and then use 9mm emery, 6mm emery, 3mm emery abrasive paste and 0.3 Millimeter emery grinding paste polishes one side of the slice, and uses water as the cooling fluid to obtain a smooth, flat and undamaged surface, and until the thickness deviation of the slice is less than 0.0...

Embodiment 2

[0037] This embodiment is aimed at the densely-mixed AC13 asphalt mixture sample, and the porosity is 4.6%. By adopting the method of the invention, the asphalt mixture ultra-thin slices with a thickness of only 0.03 mm and which can be used for microscopic analysis are successfully prepared. Aiming at the asphalt mixture super thin slices obtained by the preparation method of the present invention, it can be used for nano-probe modulus analysis, so as to obtain the modulus distribution diagram that changes with the depth of the test piece, such as image 3 Shown. image 3 In the curve on the right side, with the extension of service time, the asphalt mortar close to the surface is affected by external conditions, and the degree of aging is the most significant. Therefore, it shows a modulus distribution diagram like the black curve, that is, the closer to the road surface, the mortar The greater the modulus of the asphalt pavement; when the surface of the asphalt pavement is ...

Embodiment 3

[0039] By adopting the preparation method of the present invention, it is also possible to prepare asphalt mixture super flakes with the asphalt mixture gradation type spuperpave 12.5 and the porosity of 5.1%.

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Abstract

The invention discloses a preparation method of an asphalt mixture ultrathin slice. The preparation method comprises the following steps: 1) an asphalt mixture sample is immersed in an uncured polyester material, and gaps of the asphalt mixture sample are filled with the polyester material under the vacuum negative pressure condition so as to obtain the asphalt mixture sample filled with the polyester material; 2) the polyester material in the asphalt mixture sample filled with the polyester material is cured, and the sample is cut into a slice of less than 8 mm thick, and one side of the slice is polished until thickness deviation is less than 0.05 mm so as to obtain an asphalt mixture slice; and 3) the asphalt mixture slice obtained from the Step 2) is washed and dried and a glass sheet is pasted on the polished surface of the slice by the use of resin, and the slice is cut and polished until thickness is no more than 0.03 mm so as to obtain the asphalt mixture ultrathin slice for optical microscopic observation. The preparation method of the asphalt mixture ultrathin slice can be used for preparation of a sample applicable to microscopic structure observation of an asphalt mixture. According to the invention, research precision is raised.

Description

Technical field [0001] The invention relates to a method for preparing super thin slices of asphalt mixture specimens that can be used for microscopic observation. Background technique [0002] After long-term service, asphalt pavement is prone to pavement diseases caused by material aging. If the asphalt pavement is aging to a certain degree or the early disease appears in the early stage of pre-maintenance treatment, it can effectively inhibit the accelerated development of the disease, protect the entire road surface and extend the service life. However, in the pre-maintenance process, after the regenerant is sprayed on the asphalt pavement, its diffusion, penetration and effect in the aging asphalt mixture are not clear. At present, the research on the diffusion of regenerating agent for pavement pre-maintenance in old asphalt, the commonly used techniques such as hydrogen nuclear magnetic resonance spectrum analysis, dynamic shear performance analysis and FTIR analysis are ...

Claims

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Application Information

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IPC IPC(8): G01N1/28
CPCG01N1/286G01N2001/2873
Inventor 肖月钟赛吴少鹏王业飞孔德智万淼
Owner WUHAN UNIV OF TECH
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