A kind of preparation method of carbon fiber-polycarbonate composite material
A technology of polycarbonate and composite materials, applied in the field of carbon fiber composite materials, can solve the problems of carbon fiber materials such as high cost, high price, and small thermal expansion coefficient, and achieve the effect of reducing cost and price and improving environmental protection performance
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Embodiment 1
[0023] The preparation method of carbon fiber-polycarbonate composite material, its step is as follows:
[0024] (1), walnut shells and pine nut shells with a weight ratio of 1:1 are pulverized with a pulverizer, dried after passing through a 40-mesh sieve to obtain mixed shell powder, and the mixed shell powder is added to phosphoric acid with a concentration of 30%, and the mixed shell powder , the weight ratio of phosphoric acid is 1:6, after soaking for 2 days, suction filter, dry at 90°C for 30 hours, add to tube furnace, heat up to 180°C, keep warm for 3 hours, cool to room temperature naturally, wash with deionized water to neutral properties, dried at 90°C to constant weight to obtain mixed carbon powder;
[0025] (2) Add the mixed carbon powder obtained in step (1) into the silicon surfactant, stir for 1 hour and then add it to the melted polyester, mix at 100°C to obtain the masterbatch, add the masterbatch and polyester chips into the mixer Spinning after mixing, a...
Embodiment 2
[0028] The preparation method of carbon fiber-polycarbonate composite material, its step is as follows:
[0029] (1), walnut shells and pine nut shells with a weight ratio of 1:1 are pulverized with a pulverizer, dried after passing through a 40-mesh sieve to obtain mixed shell powder, and the mixed shell powder is added to phosphoric acid with a concentration of 30%, and the mixed shell powder , the weight ratio of phosphoric acid is 1:6, after soaking for 2 days, suction filter, dry at 90°C for 30 hours, add to tube furnace, heat up to 180°C, keep warm for 3 hours, cool to room temperature naturally, wash with deionized water to neutral properties, dried at 90°C to constant weight to obtain mixed carbon powder;
[0030] (2) Add the mixed carbon powder obtained in step (1) into the silicon surfactant, stir for 1 hour and then add it to the melted polyester, mix at 100°C to obtain the masterbatch, add the masterbatch and polyester chips into the mixer Spinning after mixing, a...
Embodiment 3
[0033] The preparation method of carbon fiber-polycarbonate composite material, its step is as follows:
[0034] (1), walnut shells and pine nut shells with a weight ratio of 1:1 are pulverized with a pulverizer, dried after passing through a 40-mesh sieve to obtain mixed shell powder, and the mixed shell powder is added to phosphoric acid with a concentration of 30%, and the mixed shell powder , the weight ratio of phosphoric acid is 1:6, after soaking for 2 days, suction filter, dry at 90°C for 30 hours, add to tube furnace, heat up to 180°C, keep warm for 3 hours, cool to room temperature naturally, wash with deionized water to neutral properties, dried at 90°C to constant weight to obtain mixed carbon powder;
[0035] (2) Add the mixed carbon powder obtained in step (1) into the silicon surfactant, stir for 1 hour and then add it to the melted polyester, mix at 100°C to obtain the masterbatch, add the masterbatch and polyester chips into the mixer Spinning after mixing, a...
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