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A rapid method for evaluating the storage stability of modified asphalt

A technology for storage stability and modified asphalt, which is applied in thermal analysis of materials, instruments, thermal conductivity of materials, etc., can solve the problems of unusable modified asphalt, unqualified storage stability, and affecting the performance of modified asphalt, and achieves a solution Unity problems, intuitive results, and easy operation

Inactive Publication Date: 2018-09-18
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Similarly, the inorganic material and asphalt material system, nano-material modified asphalt will also appear delamination, that is, the storage stability is unqualified, which will affect the performance of the modified asphalt
Modified asphalt with unqualified storage stability cannot be used in production and construction

Method used

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  • A rapid method for evaluating the storage stability of modified asphalt
  • A rapid method for evaluating the storage stability of modified asphalt
  • A rapid method for evaluating the storage stability of modified asphalt

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Mix base asphalt with 4% SBS (styrene-butadiene-styrene block copolymer) at 180°C with high shear equipment for 60 minutes to prepare polymer modified asphalt A, use base asphalt with 4% SBS (styrene-butadiene-styrene block copolymer) and 0.5% stabilizer (containing dimorpholine disulfide 35%, lead oxide 50%, carbon black 15%), polymer modified Asphalt B, take modified asphalt in a hot melt state and inject it into a test tube (the length of the test tube is 20cm, and the diameter of the tube is 25mm), place it in an oven at 163°C for 48 hours, take out the test tube sample and cool it immediately, and then separate the asphalt from the test tube. And the modified asphalt was divided into three parts of equal length, and the upper and bottom modified asphalt were taken to measure the thermal conductivity and thermal diffusivity with a thermal constant analyzer. The data obtained from the test are shown in Table 1. From the thermophysical constant method, the thermal con...

Embodiment 2

[0017] Mix base asphalt and 3% montmorillonite at 180°C with high-shear equipment for 60 minutes to prepare inorganic material modified asphalt C, use base asphalt and 3% montmorillonite, and add 0.5% stabilizer ( Calcium oxide) to prepare inorganic material modified asphalt D, take the modified asphalt in a hot melt state and inject it into a test tube (the length of the test tube is 20cm, and the diameter is 25mm), and place it in an oven at 163°C for 48h. After taking out the test tube sample, immediately After cooling, the asphalt was separated from the test tube, and the modified asphalt was divided into three parts of equal length. The modified asphalt on the upper part and the bottom part were taken to measure the thermal conductivity and thermal diffusivity with a thermal constant analyzer. The data obtained from the test are shown in Table 2. From the thermophysical constant method, we can conclude that the difference in thermal conductivity and thermal diffusivity is ...

Embodiment 3

[0021] Mix base asphalt with 8% nano-calcium carbonate at 180°C with high-shear equipment for 60 minutes to prepare nanomaterial-modified asphalt E, and use base asphalt with 8% nano-calcium carbonate and 0.5% stabilizer to prepare nano-materials Material modified asphalt F, take the modified asphalt in hot melt state and pour it into a test tube (the length of the test tube is 20cm, the diameter of the tube is 25mm), put it in an oven at 163°C for 48h, take out the sample of the test tube and cool it immediately, and then make the asphalt and The test tubes were separated, and the modified asphalt was divided into three parts of equal length. The upper and lower modified asphalt were taken to measure the thermal conductivity and thermal diffusivity with a thermal constant analyzer. The data obtained from the test are shown in Table 3. From the thermal physical constant test method, we get that the difference in thermal conductivity and thermal diffusivity is greater than 5%, w...

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Abstract

The invention relates to a method for rapid evaluation of storage stability of modified asphalt. The method comprises the following steps that the modified asphalt in a hot melting state is taken and injected in a test tube, the test tube is put in an oven and kept for 48 h at the temperature of 163 DEG C, the test tube sample is cooled immediately after being taken out, then the asphalt is separated from the test tube, the modified asphalt is divided into three parts with equal length, the upper part and the bottom part of the modified asphalt are taken, a thermal constant analysis meter is used for measuring the thermal conduction coefficient and the thermal diffusion coefficient of the upper part and the bottom part of the modified asphalt, and when the difference ratio of the thermal conduction coefficients and the difference ratio of the thermal diffusion coefficients are both smaller than or equal to 5%, it is determined that the storage stability of the modified asphalt is qualified; when the difference ratio of the thermal conduction coefficients and the difference ratio of the thermal diffusion coefficients are both larger than 5%, it is determined that the storage stability of the modified asphalt is unqualified. The method is used for evaluating the storage stability of the modified asphalt, few instruments and equipment are needed, operation is easy, convenient and flexible, time is saved (the result of a test can be obtained only in 3 min), efforts are saved, and the result is visual, accurate and reliable.

Description

technical field [0001] The invention relates to a method for rapidly and accurately evaluating the storage stability (that is, compatibility) of various modified asphalts by using thermal physical property constants. Background technique [0002] Asphalt is an important construction material, mainly used in the field of road construction. At present, in order to improve the quality of asphalt and prolong the service life of the pavement, it has become a widely implemented and effective method to modify asphalt with high molecular polymers and inorganic materials. Due to the large difference in performance between polymers and asphalt, the two are difficult to dissolve and form a stable system. Once stationary, most of the polymers will float up to form a polymer-rich polymer phase, and the lower part is asphalt. Dominated asphalt phase. Similarly, the inorganic material and asphalt material system, nano-material modified asphalt will also appear delamination phenomenon aft...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N25/18G01N25/00
CPCG01N25/00G01N25/18
Inventor 刘刚鲍远洋吴少鹏陈美祝肖月刘全涛李立平陈昊
Owner WUHAN UNIV OF TECH