A method for extracting sterenols from vegetable oil deodorization distillates
A technology of deodorizing distillates and vegetable oils, applied in the field of phytochemistry, can solve the problems of lack of single compound pesticide varieties, "pesticide pollution, poor control effect, etc., and achieve the effect of wide range of raw material sources, shortened production process, and short time
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Embodiment 1
[0048] A method for extracting sterenols from vegetable oil deodorization distillates, said method comprising the steps of:
[0049] (1) Measure 500ml in a 1000ml measuring cylinder, heat it to 60-90°C, keep it warm, then filter the deodorized distillate of cottonseed oil and 250ml of methanol through a 300-mesh screen to remove impurities, add 1000ml three-ear bottle and place it in an electric heating mantle Connect the reflux condensing device; turn on the heating, set the temperature to 65°C, turn on the stirring at the same time, adjust the speed to 80r / min, slowly drop in 20g of concentrated sulfuric acid, stop heating after 3h of reflux timing reaction, and wash with 80°C soft water to medium 485ml of reaction oil was obtained, and the sampling test showed that the acid value of reaction oil was 1.52mgKOH / g sample.
[0050] (2) Send the product washed with soft water into a multi-stage molecular distillation system for distillation, and turn on the multi-stage molecular...
Embodiment 2
[0054] The difference with Example 1 is that in step (1), pump 1000L cottonseed oil deodorization distillate and 500L methanol into the reactor, heat to 65°C and stir for 0.5h until fully dissolved; start esterification after adding 40kg of concentrated sulfuric acid catalyst Reaction: stop heating after timing for 2.5 hours, wash with soft water at 70°C three times, add 150kg of water each time, take a sample for testing, the pH value of the reaction oil is neutral after testing, and the acid value is 1.34mgKOH / g sample.
[0055] Based on the above, the method for extracting sterenols in the present invention adopts a multi-stage molecular distillation device. This process can complete decolorization, degassing, deodorization and other processes at one time, greatly shortening the production process. Under the condition of supercritical negative pressure, the material is heated evenly, the time is short, the degree of separation is high, and the temperature, vacuum degree, and...
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