High-strength composite mica paper and its preparation method
A composite mica, high-strength technology, applied in the field of mica paper, can solve the problems of inability to meet the needs of multi-field industrial applications, poor mechanical strength and toughness of mica paper, etc.
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Embodiment 2
[0026] 1) Mica flake powder (180 mesh), polyvinyl chloride-based resin (weight average molecular weight is 30,000), asbestos (thickness is 0.2mm), quaternary ammonium starch ether, ethylenediaminetetraacetic acid, water according to the weight ratio: 230:33:13:8:8:100 Stir and mix to obtain mica pulp; finally, the mica pulp is made into mica paper, and the mica paper is a mica layer; before 1), the liquid-solid ratio is 4. Wash the mica sheet with water until the turbidity of the water is 12°, and wash 3 times with water.
[0027] 2) earlier novolac epoxy resin (weight-average molecular weight is 30,000), polyimide resin (weight-average molecular weight is 40,000), ethylene glycol ether, alcohol fat twelve, dibutyl phthalate and water The mixture was mixed according to the weight ratio of 100:80:13:3:3:130, followed by heat treatment at 190° C. for 1.0 h, and finally extruded to obtain a resin layer.
[0028] 3) Place the prepared mica paper on top of the prepared resin layer...
Embodiment 3
[0030] 1) Mica flake powder (200 mesh), polyvinyl chloride-based resin (weight average molecular weight is 30,000), asbestos (thickness is 0.2mm), quaternary ammonium starch ether, ethylenediaminetetraacetic acid, water according to the weight ratio: Stir and mix at 250:35:15:10:9:100 to obtain mica pulp; finally, the mica pulp is made into mica paper, which is a mica layer; before 1), the liquid-solid ratio is Wash the mica sheet with 6 liters of water until the turbidity of the water is 10°, and wash 2 times with water.
[0031] 2) earlier novolac epoxy resin (weight-average molecular weight is 40,000), polyimide resin (weight-average molecular weight is 50,000), ethylene glycol ether, alcohol fat twelve, dibutyl phthalate and water Mixing according to the weight ratio of 100:95:15:5:5:150, followed by heat treatment at 200°C for 0.5h, and finally extrusion molding to obtain a resin layer.
[0032] 3) Place the prepared mica paper on top of the prepared resin layer, heat pr...
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