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Method for Improving the Uniformity of Microstructure and Properties of In-Situ Particle Reinforced Aluminum Matrix Composites

A particle-reinforced aluminum and composite material technology, applied in the field of materials, can solve problems such as elongation, low strength, and uneven structure of in-situ particle-reinforced aluminum-based composite materials, and achieve the goal of refining aluminum matrix grains and improving uniformity Effect

Active Publication Date: 2018-02-02
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In industrial applications, it is difficult to disperse a large number of particle agglomerates in the as-cast structure of in-situ particle reinforced aluminum matrix composites with simple unidirectional extrusion or unidirectional rolling deformation processes, and due to the traditional unidirectional extrusion With rolling, the alloy structure will be preferentially oriented, and elongated lath-like or knitted dendrites will be formed in the aluminum matrix, thereby making the structure of the in-situ particle-reinforced aluminum matrix composite extremely inhomogeneous.
Such an inhomogeneous structure will also make the performance of in-situ particle reinforced aluminum matrix composites show obvious anisotropy. Direction, low strength, poor plasticity
The above-mentioned anisotropy of microstructure and properties severely limits the application of in-situ particle-reinforced aluminum matrix composites in industrial production, and is also an urgent problem for material scientists and technicians.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] In situ self-generated 5wt.%TiB obtained by casting 2 / 7075Al composite material, its as-cast grain structure is coarse, a large amount of TiB 2 Particles agglomerate at grain boundaries. In situ self-generated 5wt.%TiB obtained by casting 2 / 7075Al composite material was homogenized at 465°C for 24 hours, and then subjected to unidirectional extrusion deformation at 450°C (extrusion ratio 10:1). After extrusion, the matrix grain structure was deformed along the extrusion direction Elongated to present lath-shaped or knitted branches, TiB obtained by casting 2 Particle agglomerates are also stretched along the grains and are still distributed at a large number of grain boundaries. Such an inhomogeneous structure also leads to in situ autogenous 5wt.%TiB after unidirectional extrusion 2 The / 7075Al composite exhibits severe anisotropy, with a tensile strength of 717MPa and a fracture plasticity of 9.6% along the extrusion direction, and a tensile strength of 625MPa p...

Embodiment 2

[0022] In situ self-generated 5wt.%TiB obtained by casting 2 / 2024Al composite material, consistent with Example 1, in the cast state and simple extrusion state, the structure and mechanical properties of the composite material are extremely inhomogeneous, showing obvious anisotropy, and the composite material has a higher Strength and certain plasticity, but in the direction perpendicular to the extrusion, the strength of the composite material decreases, and there is almost no plasticity. Therefore, according to the technical scheme of the present invention, the in-situ self-generated 5wt.%TiB 2 / 2024Al composites were subjected to unidirectional extrusion deformation at 450°C after homogenizing the alloying elements at 490°C for 48h (extrusion ratio 16:1). 5wt.%TiB after unidirectional extrusion 2 / 2024Al composite material, rolling along the direction perpendicular to the extrusion, the rolling temperature is 450 ℃, each rolling deformation is 10%, after the rolling is c...

Embodiment 3

[0024] A method for improving the uniformity of microstructure and properties of in-situ particle reinforced aluminum matrix composites, the following steps are adopted:

[0025] (1) The in-situ authigenic casting containing 1wt% TiB 2 The 2xxx series composite materials are subjected to homogenization heat treatment of alloying elements at 465°C for 72h;

[0026](2) The homogenized in-situ particle-reinforced aluminum matrix composite material is subjected to unidirectional hot extrusion deformation, the temperature is controlled at 300°C, and the hot extrusion ratio is greater than or equal to 10:1;

[0027] (3) The hot-extruded in-situ particle-reinforced aluminum-based composite material is hot-rolled, the rolling direction is perpendicular to the unidirectional hot-extrusion direction, the rolling temperature is 300°C, and the deformation per rolling is less than or equal to 10 %, after the rolling is completed, the reduction in the total height of the composite material...

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Abstract

The invention relates to a method for improving the uniformity of the microstructure and performance of in-situ particle reinforced aluminum-based composite materials. The particle-reinforced aluminum-based composite material obtained by in-situ autogenous casting is subjected to homogenization heat treatment of alloy elements; the homogenized in-situ particle The reinforced aluminum matrix composite is subjected to unidirectional hot extrusion deformation; the hot-extruded in-situ particle-reinforced aluminum-matrix composite is hot-rolled; the rolled in-situ particle-reinforced aluminum-matrix composite is subjected to T6 heat treatment, namely Finish processing. The invention adopts two-step orthogonal thermal deformation, which is beneficial to break up the agglomeration of self-generated ceramic particles in the in-situ particle reinforced aluminum matrix composite material, and obtain a uniformly dispersed ceramic reinforcement phase, and through unidirectional extrusion and orthogonal rolling phase Combined, it can effectively refine the grains of the aluminum matrix and prepare a finer and equiaxed matrix grain structure, thereby improving the uniformity of the microstructure and properties of the in-situ particle-reinforced aluminum matrix composite.

Description

technical field [0001] The invention belongs to the field of material technology, and in particular relates to a method for improving the uniformity of structure and performance of in-situ particle reinforced aluminum-based composite materials. Background technique [0002] With the development of modern science and technology, the requirements for material properties in practical applications have become more stringent. Especially in high-tech fields such as aerospace and weapon manufacturing, structural materials should have high specific stiffness and specific modulus while requiring high strength and high plasticity. However, traditional metal materials are difficult to meet such complex performance requirements. For example, although traditional steel materials have good strength and plasticity, their density is too high, so they are not suitable for a large number of applications in aerospace and other fields that have high requirements for specific strength of compon...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/04C22C1/10
CPCC22C1/1036C22F1/002C22F1/04C22C1/1047
Inventor 陈哲刘钧汪明亮吴一陈东钟圣怡王浩伟
Owner SHANGHAI JIAO TONG UNIV
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