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Microreactor with replaceable bed layer and application of microreactor

A microreactor and bed technology, applied in the field of energy and chemical industry, can solve the problems of poor heat transfer performance, difficult operation, troublesome catalyst loading and replacement, etc., and achieve the effects of improving utilization rate, convenient operation, and promoting combination.

Inactive Publication Date: 2017-01-11
SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In view of the above-mentioned shortcoming of prior art, the object of the present invention is to provide a kind of microreactor and application thereof that can replace the bed, be used to solve the poor heat transfer performance of the reactor adopting fixed bed mode in the prior art, catalyst It is troublesome to load and replace the catalyst; for microreactors using the coating method, the replacement and unloading process of the catalyst is difficult, the operation is difficult, and the bed cannot be reused, etc.

Method used

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  • Microreactor with replaceable bed layer and application of microreactor
  • Microreactor with replaceable bed layer and application of microreactor
  • Microreactor with replaceable bed layer and application of microreactor

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Embodiment 1

[0055] The present invention provides a microreactor with replaceable bed, please refer to figure 1 and figure 2 , which are respectively shown as the disassembled structure schematic diagram and the assembled side view of the microreactor of the replaceable bed, including the upper cover plate 1, the lower cover plate 2 and the upper cover plate 1 and the lower cover plate 2 sandwiched between The microreactor base layer 3.

[0056] As an example, the upper cover plate 1 , the lower cover plate 2 and the microreactor base layer 3 sandwiched between the upper cover plate and the lower cover plate are connected by fasteners. In this embodiment, the fastener includes at least two bolts 4 ( figure 1 In the case of eight bolts shown in ), the upper cover plate 1 , the lower cover plate 2 and the microreactor base layer 3 are all provided with mounting holes 5 that match the bolts 4 .

[0057]Specifically, a sealing ring 6 is provided between the upper cover plate 1 and the mic...

Embodiment 2

[0080] The invention also provides an application of the microreactor. The application is to carry out the Fischer-Tropsch synthesis reaction in the microreactor adopting the replaceable bed layer described in Example 1.

[0081] Fischer-Tropsch synthesis (Fischer-Tropsch synthesis) is one of the most important synthesis reaction systems in the field of coal chemical industry, which can be referred to as FT reaction. 2 ) as a raw material to synthesize a variety of important industrial raw materials such as alkanes, olefins, alcohols, etc. under catalysts (mainly iron series) and appropriate reaction conditions.

[0082] As an example, the operation method of the replaceable bed microreactor of the present invention is as follows: firstly open a path of hydrogen to feed into the reactor, adjust to a suitable temperature and pressure to carry out the reduction process of the catalyst. After the reduction for an appropriate time, the reaction raw material gas hydrogen and carbo...

Embodiment 3

[0086] The present invention also provides an application of a microreactor, which is to convert carbon dioxide into methanol in the microreactor adopting the replaceable bed described in the first embodiment.

[0087] Specifically, a mixed gas of carbon dioxide and hydrogen is used as a raw material gas, and metal ruthenium is used as a catalyst, and heated to a suitable temperature so that the reaction proceeds, and the carbon dioxide is converted into methanol. The specific operation method is similar to the first embodiment, and will not be repeated here.

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Abstract

The invention provides a microreactor with a replaceable bed layer and application of the microreactor. The microreactor comprises an upper cover plate, a lower cover plate and a microreactor substrate layer clamped between the upper cover plate and the lower cover plate; a raw material gas preheating channel, a raw material gas distribution structure, a cavity structure for accommodating a catalyst bed layer and a tail gas collecting structure which are sequentially connected are arranged in the microreactor substrate layer; a gas inlet and a gas outlet are formed in the upper cover plate; the gas inlet is communicated with a gas inlet of the raw material gas preheating channel; the gas outlet is communicated with a gas outlet of the tail gas collecting structure. According to the microreactor provided by the invention, by adopting a design method of separating the catalyst bed layer at a reaction site from the microreactor substrate layer, the replacement cost of a catalyst can be reduced; the microreactor is suitable for a mode of combining multiple catalysts; the reaction intensifying process is effectively realized, the reaction conversion rate is improved, and industrial application of the microreactor is facilitated.

Description

technical field [0001] The invention belongs to the field of energy and chemical industry, and relates to a micro-reactor with a replaceable bed layer and its application. Background technique [0002] Fischer-Tropsch synthesis reaction is one of the most important synthesis reaction systems in the field of coal chemical industry. The reaction system uses synthesis gas as a raw material, and can produce various important industrial raw materials such as alkanes, olefins, and alcohols. Since syngas can be produced from coal, the Fischer-Tropsch reaction has important strategic significance for countries with more coal and less oil. [0003] Currently, Fischer-Tropsch synthesis reactions mainly include fixed bed, fluidized bed, and microchannel reactors. The fixed-bed reactor is simple in construction, low in cost and easy to operate, but has disadvantages such as heat transfer, poor mixing effect, and inability to replace the catalyst on-line. Compared with the fixed bed r...

Claims

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Application Information

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IPC IPC(8): B01J19/00B01J8/02C10G2/00C07C1/12C07C9/04C07C29/152C07C31/04
CPCB01J19/0093B01J2219/00781B01J2219/00783B01J2219/00873C07C1/12C07C29/152C10G2/34C10G2/341C07C9/04C07C31/04Y02P20/141Y02P20/52
Inventor 孙予罕梁庄典吕敏唐志永
Owner SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI
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