Method for producing natural gas through methanation of synthesis gas by virtue of Raney alloy catalyst
A technology for natural gas and catalyst, which is applied in the field of Raney alloy catalyst for synthesis gas methanation to natural gas, and can solve the problems of low carbon oxide conversion rate and the like
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Embodiment 1
[0042] This example is used to illustrate the method for producing natural gas by methanation of synthesis gas provided by the present invention.
[0043] (1) Preparation of catalyst
[0044] a, polyethylene glycol stearate (Jiahua Chemical, PEG400MS) 80g, curing agent methyltetrahydrophthalic anhydride (MeTHPA) (Guangdong Shengshida Technology and Trade Co., Ltd.) 68g, curing accelerator triethanolamine (TEA) (Tianjin Chemical Reagent No. 1 Factory) 1.2g was stirred evenly.
[0045] B, take by weighing 50g solidification system prepared in step (1), drop it in the cylindrical mold that has added part nickel-aluminum alloy powder with dropper, nickel content is 48% by weight in the nickel-aluminum alloy, and aluminum content is 52% % by weight, then fill the mold with nickel-aluminum alloy powder, put it into a flat vulcanizer, mold it for 30min under the conditions of temperature 120°C and pressure 7MPa, take out the particles, place them in nickel-aluminum alloy powder, and...
Embodiment 2
[0052] This example is used to illustrate the method for producing natural gas by methanation of synthesis gas provided by the present invention.
[0053] (1) Preparation of catalyst
[0054] a. Fully mix liquid epoxy resin (Baling Petrochemical, CYD-128) and curing agent hexamethylenetetramine with a high-speed mixer. The weight ratio of hexamethylenetetramine to liquid epoxy resin is 12:100; 100 grams of compound material and 300 grams of nickel-aluminum alloy powder are fully mixed with a high-speed mixer, and the nickel content in the nickel-aluminum alloy powder is 48% by weight, and the aluminum content is 52% by weight;
[0055] b. Raise the temperature of the tablet press to 90°C, put the above materials into the mold and press on the tablet press to form a sheet with a thickness of 2mm; raise the temperature of the tablet press to 150°C, and place the formed sheet again Enter the mold and solidify under the pressure of 5MPa on the tablet press for 10min;
[0056] c....
Embodiment 3
[0063] This example is used to illustrate the method for producing natural gas by methanation of synthesis gas provided by the present invention.
[0064] (1) Preparation of catalyst
[0065] a, polyethylene glycol stearate (Jiahua Chemical, PEG400MS) 80g, curing agent methyltetrahydrophthalic anhydride (MeTHPA) (Guangdong Shengshida Technology and Trade Co., Ltd.) 68g, curing accelerator triethanolamine (TEA) (Tianjin Chemical Reagent No. 1 Factory) 1.2g was stirred evenly.
[0066] B, take by weighing 50g solidification system prepared in step (1), drop it in the cylindrical mold that has added part nickel-aluminum alloy powder with dropper, nickel content is 48% by weight in the nickel-aluminum alloy, and aluminum content is 52% % by weight, then fill the mold with nickel-aluminum alloy powder, put it into a flat vulcanizer, mold it for 30min under the conditions of temperature 120°C and pressure 7MPa, take out the particles, place them in nickel-aluminum alloy powder, and...
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