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A new processing method and device for producing polyvinyl alcohol powder

A technology of polyvinyl alcohol powder and processing method, applied in separation methods, chemical instruments and methods, filtration separation and other directions, can solve problems such as environmental pollution, potential safety hazards, increased methanol consumption, etc., and achieve the effect of reducing production costs

Active Publication Date: 2019-12-06
SINOPEC CHANGCHENG ENERGY CHEM NINGXIA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In order to ensure product quality, the PVA powder in the sedimentation tank is currently discharged from the manhole and discharge port during maintenance, which is labor-intensive and time-consuming, resulting in increased methanol consumption, unqualified wastewater discharge, and potential safety hazards
The PVA powder discharged from the mother liquor filter is too wet and contains methanol, which is not conducive to bagging, storage and sales. The PVA powder discharged from the mother liquor filter is used as waste in the production process of polyvinyl alcohol, and has been stored in the open until a certain amount is sold. Methanol is highly volatile, and the concentration of methanol in the storage location is high. In addition to potential safety hazards, it will also cause environmental pollution

Method used

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  • A new processing method and device for producing polyvinyl alcohol powder

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Embodiment Construction

[0012] Specific embodiments of the present invention are described with reference to the drawings.

[0013] Such as figure 1 Shown: a new processing method and device for producing polyvinyl alcohol powder, the device includes an alcoholysis machine 1, a first pulverizer 2, a second pulverizer 3, an extruder 4, a dryer 5, and a screw conveyor 6. Vibrating screen 7. Unpacking silo air delivery pipeline 8. Sedimentation tank 9. Distribution liquid adding pump 10. Mother liquor sending pump 11. Cyclone separator 12. Mother liquor filter 13. Hot water adding pipeline 14. Nitrogen gas adding pipeline 15 , stock solution tank 16, methanol condensation tower 17, by-product dryer 18, by-product screw conveyor 19, by-product vibrating screen 20, packaging machine 21, by-product centrifuge 22a, product centrifuge 22b, filtrate to tank area stock solution storage tank pipeline 23, Filter cake packaging or by-product removal dryer pipeline 24, defoamer storage tank 25, defoamer adding pu...

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Abstract

The invention relates to a novel processing method and device for producing polyvinyl alcohol powder and belongs to the field of polyvinyl alcohol production. The method includes: PVA powder mother liquor generated after alcoholysis during polyvinyl alcohol production enters a precipitation tank from an alcoholysis machine and an extruder, is stirred by the precipitation tank and enters a mother liquor filtering machine, the solid-liquid mixture in the filtering machine is fed into a byproduct centrifuge to perform solid-liquid separation, solid is fed into a drying machine for drying, and packaging is performed. The device comprises the alcoholysis machine, a crusher, the extruder, the drying machine, a spiral conveyor, a vibration screen, a stock bin pneumatic conveying pipeline, the precipitation tank, a distribution liquid adding pump, a mother liquor delivering pump, a cyclone separator, a mother liquor filtering machine, a stock solution tank, a methanol condensing tower, a byproduct drying machine, a byproduct conveyor, a vibration screen, a packaging machine, the byproduct centrifuge, a centrifuge, a defoaming agent storage tank and a defoaming agent adding pump which are connected through pipelines. By the novel processing method and device, polyvinyl alcohol production cost is lowered, environment pollution is reduced, and potential safety hazard is eliminated.

Description

technical field [0001] The invention belongs to the technical field of polyvinyl alcohol production, in particular to a method and device for processing PVA powder in the production process of polyvinyl alcohol. Background technique [0002] In the existing production process of polyvinyl alcohol, the alcoholysis unit mother liquor process is as follows: the alcoholysis mother liquor extruded by the screw extruder contains a small amount of PVA powder, and after entering the sedimentation tank, the PVA powder is precipitated and settles down at the bottom of the sedimentation tank The PVA powder is sent back to the inlet of the screw extruder through the distribution liquid pump to recover the PVA therein. The supernatant liquid in the sedimentation tank is sent to the alcoholysis mother liquor storage tank in the intermediate tank area after being filtered by the mother liquor delivery pump and the mother liquor filter. At present, the two columns of the sedimentation tank...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D36/04C08L29/04
CPCB01D36/045C08L29/04
Inventor 唐玉林
Owner SINOPEC CHANGCHENG ENERGY CHEM NINGXIA CO LTD
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