Preparation method of caterpillar fungus concentration solution
A preparation method and a technology for a concentrated solution are applied in the production field of a concentrated solution of Cordyceps militaris, and can solve the problems such as many impurities in the concentrated solution, and achieve the effect of less impurities
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Embodiment 1
[0022] A preparation method of a concentrated solution of Cordyceps militaris, comprising the steps of:
[0023] 1) Raw material processing: Dried the body of Cordyceps militaris, chopped it, and soaked it with ethanol solution A for 15 minutes to obtain the soaked Cordyceps militaris; the mass concentration of the ethanol solution A was 35%;
[0024] 2) Percolation: Put the infiltrated Cordyceps militaris into the percolation tank; add A ethanol solution to soak for 15 hours; percolate the mixture in the percolation tank, and maintain a certain percolation speed, the percolation rate is 10 ml per Minutes, get percolate;
[0025] 3) Reflux concentration: put the percolation liquid in a reaction tank, recover ethanol under reduced pressure, and obtain concentrated liquid A;
[0026] 4) Alcohol precipitation: add B ethanol solution to concentrated solution A until the mass concentration of ethanol reaches 60%, and the mass concentration of B ethanol solution reaches 90%; after ...
Embodiment 2
[0029] A preparation method of a concentrated solution of Cordyceps militaris, comprising the steps of:
[0030] 1) Raw material processing: Dried the body of Cordyceps militaris, chopped it, soaked it with A ethanol solution for 45 minutes, and obtained the infiltrated Cordyceps militaris; the mass concentration of A ethanol solution was 45%;
[0031] 2) Percolation: Put the infiltrated Cordyceps militaris into the percolation tank; add A ethanol solution to soak for 30 hours; percolate the mixture in the percolation tank, and maintain a certain percolation speed, the percolation rate is 20 ml per Minutes, get percolate;
[0032] 3) Reflux concentration: put the percolation liquid in a reaction tank, recover ethanol under reduced pressure, and obtain concentrated liquid A;
[0033] 4) Alcohol precipitation: Add B ethanol solution to concentrated solution A until the mass concentration of ethanol reaches 80%, and the mass concentration of B ethanol solution is 98%; after stir...
Embodiment 3
[0036] A preparation method of a concentrated solution of Cordyceps militaris, comprising the steps of:
[0037] 1) Raw material processing: Dried the body of Cordyceps militaris, chopped it, soaked it with ethanol solution A for 30 minutes, and obtained the soaked Cordyceps militaris; the mass concentration of the ethanol solution A was 40%;
[0038] 2) Percolation: put the infiltrated Cordyceps militaris into the percolation tank; add A ethanol solution to soak for 24 hours; percolate the mixture in the percolation tank, and maintain a certain percolation speed, the percolation rate is 15 ml per Minutes, get percolate;
[0039] 3) Reflux concentration: put the percolation liquid in a reaction tank, recover ethanol under reduced pressure, and obtain concentrated liquid A;
[0040] 4) Alcohol precipitation: Add B ethanol solution to concentrated solution A until the mass concentration of ethanol reaches 70%, and the mass concentration of B ethanol solution reaches 95%; after ...
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