System and method for processing coarse titanium tetrachloride

A technology of crude titanium tetrachloride and titanium tetrachloride, which is applied to titanium tetrachloride, titanium halide and other directions, can solve the problems of large fluctuation in the quality of refined titanium tetrachloride, waste of industrial raw materials and materials, and increase of production costs.

Inactive Publication Date: 2017-05-31
YUNNAN METALLURGICAL XINLI TITANIUM IND CO LTD
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Problems solved by technology

[0003] At present, due to the different and imperfect refining processes, the mixing effect of crude titanium tetrachloride and mineral oil in the production process is not good, resulting in poor vanadium removal effect of crude titanium tetrachloride and refined tetrachloride after vanadium removal. The quality of titanium chloride fluctuates greatly, frequent pipeline and equipment blockages cause discontinuous production, frequent equipment and pipeline maintenance, resulting in waste of industrial raw materials and mat

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  • System and method for processing coarse titanium tetrachloride
  • System and method for processing coarse titanium tetrachloride
  • System and method for processing coarse titanium tetrachloride

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[0037] The embodiments of the present invention will be described in detail below. Examples of the embodiments are shown in the accompanying drawings, wherein the same or similar reference numerals indicate the same or similar elements or elements with the same or similar functions. The embodiments described below with reference to the accompanying drawings are exemplary, and are intended to explain the present invention, but should not be construed as limiting the present invention.

[0038] In the present invention, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", "fixed" and other terms should be understood in a broad sense, for example, it may be a fixed connection or a detachable connection , Or integrated; it can be mechanically connected or electrically connected; it can be directly connected or indirectly connected through an intermediary, it can be the internal communication of two components or the interaction relationship ...

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Abstract

The invention discloses a system and a method for processing coarse titanium tetrachloride. The system comprises a mixing tank, an evaporator, a buffering tank, a vanadium slag pump and a vanadium slag recovering device, wherein the mixing tank is provided with a coarse titanium tetrachloride inlet, an organic matter inlet and a mixture outlet; a stirrer is arranged in the mixing tank; the evaporator is provided with a mixture inlet, a steam inlet, a fine titanium tetrachloride gas outlet and a vanadium slag outlet; another stirrer is arranged in the evaporator; the buffering tank is provided with a vanadium slag inlet and a vanadium slag discharging port; the vanadium slag pump is connected with the vanadium slag discharging port; and the vanadium slag recovering device is connected with the vanadium slag pump. With the adoption of the system, the average blocking times of a vanadium slag pipeline are reduced to be once a month; the perforating times of the vanadium slag pump are reduced to be once every three months; in addition, the yield of obtained fine titanium tetrachloride is beyond 95%; and compared with the prior art, the yield of fine titanium tetrachloride is increased by more than 18-35%.

Description

Technical field [0001] The present invention belongs to the field of chemical industry. Specifically, the present invention relates to a system and method for processing crude titanium tetrachloride. Background technique [0002] At present, in the production process of titanium dioxide produced by the chloride method, the crude titanium tetrachloride produced needs to be refined, and the refining is mainly to remove the vanadium in the crude titanium tetrachloride. The existing refining processes mainly include the removal of vanadium from copper wire, the removal of vanadium from aluminum powder, and the removal of vanadium from organic matter. The specific implementation process is selected according to economic benefits and needs. For the production of titanium dioxide by the chlorination method, organic matter is mainly used to remove vanadium, and the selected organic matter is oil. Through the reducibility of the oil, the vanadium in the crude titanium tetrachloride genera...

Claims

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Application Information

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IPC IPC(8): C01G23/02
CPCC01G23/024
Inventor 冯炜光江书安吉立明李保金龚如竟普建国钱春花
Owner YUNNAN METALLURGICAL XINLI TITANIUM IND CO LTD
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