Process for preparing branched chain amino acid and application of process
A branched-chain amino acid and process technology, which is used in the preparation of cyanide reactions, the preparation of organic compounds, and medical preparations containing active ingredients, etc. It can solve the problem of regenerated acid and alkali, and achieve the effect of solving the amount of regenerated acid and alkali and salt pollution, reducing waste water discharge and reducing acid and alkali consumption.
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Embodiment 1
[0054] A process for preparing branched-chain amino acids, said process comprising the steps of:
[0055] Step 1, raw material pretreatment;
[0056] Step 2, preparation of crude branched-chain amino acid;
[0057] Step 3, organic-inorganic composite membrane purification;
[0058] Step 4, low temperature concentration and crystallization;
[0059] Step five, low temperature vacuum microwave drying;
[0060] Step six, crushing;
[0061] Step 7, infrared-microwave drying;
[0062] Step eight, packing.
[0063] The specific steps of the raw material pretreatment are:
[0064] Step 1), preparation of branched-chain amino acid fermentation liquid;
[0065] Step 2), preparation of ion exchange resin;
[0066] Step 3), preparation of microfiltration membrane, ultrafiltration membrane and reverse osmosis membrane filter;
[0067] Step 4), preparation of organic-inorganic composite membrane.
[0068] The preparation of the crude branched-chain amino acid specifically include...
Embodiment 2
[0090] A process for preparing branched-chain amino acids, said process comprising the steps of:
[0091] Step 1, raw material pretreatment;
[0092] Step 2, preparation of crude branched-chain amino acid;
[0093] Step 3, organic-inorganic composite membrane purification;
[0094] Step 4, low temperature concentration and crystallization;
[0095] Step five, low temperature vacuum microwave drying;
[0096] Step six, crushing;
[0097] Step 7, infrared-microwave drying;
[0098] Step eight, packing.
[0099] The specific steps of the raw material pretreatment are:
[0100] Step 1), preparation of branched-chain amino acid fermentation liquid;
[0101] Step 2), preparation of ion exchange resin;
[0102] Step 3), preparation of microfiltration membrane, ultrafiltration membrane and reverse osmosis membrane filter;
[0103] Step 4), preparation of organic-inorganic composite membrane.
[0104] The preparation of the crude branched-chain amino acid specifically include...
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