Device and method for evaluating saturation capacity of moveable oil in shale

An evaluation method, shale technology, applied in the direction of measuring devices, test sample preparation, sampling, etc., can solve the problem of not being able to represent the developable oil reserves of movable oil, affecting oil and water saturation, and being unable to determine oil and water, etc. problem, to achieve the effect of shortening the experimental cycle, speeding up self-priming, and reliable data

Inactive Publication Date: 2017-06-13
CHINA UNIV OF PETROLEUM (EAST CHINA)
View PDF10 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Only after clarifying the content of crude oil in the shale in the free state, adsorption and dissolved state, can the development plan be established in a targeted manner. The current patent reports or documents are all focused on the characterization of the total porosity and organic porosity of shale. The existence of pores in shale provides a place for oil storage, but it can only represent the possible amount of oil reserves in shale, not the movable oil or developable oil reserves, which is more important for the design and selection of development plans The guiding significance is the reserves of movable oil in different occurrence states, but there is no literature or patent report related technology or method to quantify the movable oil in shale in free state and adsorption and dissolution state representation of
The prior art also provides a method for quantitatively controlling the amount of movable oil in the oil-water imbibition

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Device and method for evaluating saturation capacity of moveable oil in shale
  • Device and method for evaluating saturation capacity of moveable oil in shale
  • Device and method for evaluating saturation capacity of moveable oil in shale

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0094] Select the crushed sample 1 after oil washing and drying, weigh a sample with a mass of 46.76g, and add it to the airtight sample tank 1. The density of the sample is 2.21g / cm 3 , V 样 21.16cm 3 , through experiments, the initial and final volumes of the liquid in the first scale tube are 100.00 and 65.26 cm respectively 3 , the initial and final volumes of the liquid in the second graduated tube are 100.00 and 64.18 cm, respectively 3 , therefore, it can be calculated that the saturated amount ω′ of the alkane existing in the free state and the saturated amount ω″ of the alkane existing in the adsorbed dissolved state in the sample 1 are respectively 0.041 cm 3 / g and 0.023cm 3 / g.

Embodiment 2

[0096] Select the broken sample 2 that has been washed and dried, weigh a sample with a mass of 63.5g, and add it to a closed sample tank. The density of the sample is 2.42g / cm 3 , V 样 26.2cm 3 , through experiments, the initial and final volumes of the liquid in the first scale tube are 100.00 and 70.22 cm respectively 3 , the initial and final volumes of the liquid in the second graduated tube are 100.00 and 69.43 cm, respectively 3 , therefore, it can be calculated that the saturated amount ω′ of the alkane existing in the free state and the saturated amount ω″ of the alkane existing in the adsorbed dissolved state in the sample two are 0.031 cm 3 / g and 0.012cm 3 / g.

Embodiment 3

[0098] Select the broken sample three that has been washed and dried, weigh a sample with a mass of 45.2g, and add it to a closed sample tank. The density of the sample is 2.34g / cm 3 , V 样 19.32cm 3 , the initial and final volumes of the liquid in the first scale tube are obtained through experiments to be 10.00 and 63.86 cm respectively 3 , the initial and final volumes of the liquid in the second graduated tube are 100.00 and 63.08 cm, respectively 3 , therefore, it can be calculated that the saturation amount ω′ of the alkane existing in the free state and the saturation amount ω″ of the alkane existing in the adsorbed dissolved state in the sample three are respectively 0.032cm 3 / g and 0.017cm 3 / g.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a device for evaluating saturation capacity of moveable oil in shale. The device comprises an airtight sample tank, a sample tank cover, a first graduated tube, a second graduated tube, a vacuum pump, a four-way valve, a communicating port, a first pipeline, a second pipeline, a third pipeline, a fourth pipeline, a first stop valve, a second stop valve, a third stop valve and a fourth stop valve, wherein the sample tank cover is arranged above the airtight sample tank; the communicating port is formed in the sample tank cover; one end of the first pipeline is communicated with the airtight sample tank while the other end is communicated with the four-way valve; the first stop valve is arranged on the first pipeline; the first graduated tube is connected with the four-way valve through the second pipeline; the second stop valve is arranged on the second pipeline; the second graduated tube is connected with the four-way valve through the third pipeline; the third stop valve is arranged on the third pipeline; the vacuum pump is connected with the four-way valve through the fourth pipeline; the fourth stop valve is arranged on the fourth pipeline. The broken sample is used by the device; the efficiency is increased; the two graduated tubes are used for respectively injecting KCl solution and alkane; the pollution in an experimental process is reduced; the result is accurate.

Description

technical field [0001] The invention relates to the field of petroleum engineering and technology, in particular to a device and method for evaluating the saturation of movable oil in shale. Background technique [0002] With the in-depth study of shale gas theory and the rapid development of exploration and development, shale oil has also received extensive attention and high attention in recent years. As a sibling of shale gas, shale oil also has a relatively wide distribution. In the United States, shale oil production has increased rapidly since 2005, reaching 29.73 million tons in 2011, which has become the focus of unconventional oil and gas exploration and development. In addition, Canada and other countries have also made breakthroughs in shale oil exploration and development to varying degrees. [0003] my country is rich in shale oil resources. Since the 1960s, "shale fractured reservoirs" have been discovered in different oil and gas-bearing basins. With the de...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): G01N7/04G01N1/28
CPCG01N1/286G01N7/04
Inventor 宫厚健张少杰桑茜李亚军董明哲王宏前徐龙朱超凡张浩尚胜祥邹洪俊
Owner CHINA UNIV OF PETROLEUM (EAST CHINA)
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products