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Detection method of total phosphorus content in water

A detection method and technology for phosphorus content, which are used in measurement devices, preparation of test samples, color/spectral property measurement, etc., can solve the problems of complicated and complicated operations, severe operating conditions, and large experimental errors, and achieve a high safety factor. , The method is simple and easy to control, and the effect of high accuracy

Inactive Publication Date: 2017-06-13
GUIGANG BATIAN ECOLOGY
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Problems solved by technology

[0007] The purpose of the present invention is to provide a detection method of total phosphorus content in water quality, aiming to solve the problem of cumbersome and complicated operation, large experimental error, poor reproducibility, high risk factor and difficult operation when detecting total phosphorus content in water quality in the prior art. Strict conditions; or high cost and poor accuracy

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  • Detection method of total phosphorus content in water
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Embodiment Construction

[0020] In order to make the technical problems, technical solutions and beneficial effects to be solved by the present invention clearer, the present invention will be further described in detail below in conjunction with the embodiments. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

[0021] The embodiment of the present invention provides a kind of detection method of total phosphorus content in water quality, comprises the following steps:

[0022] (1) adopt spectrophotometry to measure the absorbance of phosphate standard solution, draw work curve;

[0023] (2) provide the water body sample to be checked, add potassium persulfate solution in the water body sample to be checked, carry out microwave sealed digestion, all the total phosphorus in the water body sample to be checked is oxidized to orthophosphate, obtain Digestion solution;

[0024] (3) Add ascorbic acid ...

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Abstract

The invention provides a detection method of total phosphorus content in water. The detection method comprises the following steps: (1) determining the absorbance of a phosphate standard solution by adopting a spectrophotometric method and drawing a working curve; (2) providing a water body test sample to be detected and adding a potassium persulfate solution into the water body test sample to be detected; carrying out microwave sealed digestion; oxidizing all total phosphorus in the water body test sample to be detected into orthophosphate, so as to obtain a digestion solution; (3) adding ascorbic acid into the digestion solution and uniformly mixing for 30s to 60s; adding a molybdate solution and carrying out color development reaction to obtain a reaction solution; (4) providing a blank water sample and referring to operation of steps (2) and (3) to obtain a blank reaction solution; (5) carrying out spectrophotometric absorbance determination on the reaction solution and the blank water sample to obtain test sample absorbance and blank absorbance respectively; referring to the working curve and calculating to obtain the total phosphorus content in the water body test sample to be detected.

Description

technical field [0001] The invention belongs to water body detection methods, in particular to a detection method for total phosphorus content in water quality. Background technique [0002] At present, in order to protect water quality and control hazards, sewage treatment has been put on the agenda as an important issue for national development both at home and abroad. Phosphorus is an important indicator to reflect the degree of water pollution and eutrophication, and it is also one of the main indicators for my country to implement the total amount of pollutant discharge control. In recent years, with the improvement and strengthening of national environmental protection laws and regulations, strict monitoring of pollutant indicators including total phosphorus in various types of wastewater and river water is required. Therefore, the research on the fast, accurate and simple method of total phosphorus in sewage and the formulation and monitoring of total phosphorus dete...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/31G01N1/44G01N1/28
CPCG01N1/28G01N1/44G01N21/31G01N2021/3185G01N2021/3196
Inventor 陈燕文陈阅梦黄德明田小山冷为贵余桂兵
Owner GUIGANG BATIAN ECOLOGY
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