A kind of consolidatable foam plugging agent
A foaming agent and blocking agent technology, applied in chemical instruments and methods, drilling compositions and other directions, can solve the problems of high cost, difficulty in forming effective blocking strength, etc., and achieve low cost, simple and safe production, and sealing. Strong blocking effect
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preparation example Construction
[0041] The preparation method of the condensable foaming plugging agent of the present invention comprises the following steps,
[0042] 1) Preparation of foaming agent aqueous solution: according to the ratio of raw materials, dissolve the foaming reaction raw materials ammonium chloride and sodium nitrite into tap water, and stir evenly at a low speed of 200 rpm for 20 minutes;
[0043] 2) Prepare epoxy resin low-viscosity solution: according to the ratio of raw materials, mix low-viscosity crude oil, triethylenetetramine, and surfactant in the epoxy resin in sequence, and stir evenly at a low speed of 200 rpm for 20 minutes;
[0044] 3) Preparation of emulsion type epoxy resin: Stir at a low speed of 200 rev / min for the epoxy resin low-viscosity solution prepared in step 2), add the foaming agent aqueous solution prepared in step 1) dropwise during the stirring process, and after the dropwise addition is completed, airtightly stir tank, and stir at a high speed of 8000 rpm ...
Embodiment 1
[0046] Raw materials (both commercially available industrial products): 30 kg of epoxy resin, 30 kg of low-viscosity crude oil, 5 kg of triethylenetetramine, 2.7 kg of ammonium chloride, 3.4 kg of sodium nitrite, 10 kg of tap water, surface Active agent 0.5 kg. The product of the present invention, the consolidated foaming plugging agent, is obtained strictly according to the preparation method described above. As the surfactant, Span-80 was used.
[0047] Indoor medium and low permeability artificial core plugging simulation test comparison: prepared permeability 220×10 -3 μm 2 The artificial cylindrical core has an outer diameter of 25.5mm and a core length of 200.4mm. Use a peristaltic pump to inject the consolidatable foaming plugging agent at a rate of 2mL / min, with an injection volume of 0.8PV and an injection permeability of 220×10 -3 μm 2 artificial core. The breakthrough pressure of the artificial core was tested to be 2.4 MPa after the artificial core was solid...
Embodiment 2
[0049]Raw materials (both commercially available industrial products): 50 kg of epoxy resin, 50 kg of low-viscosity crude oil, 10 kg of triethylenetetramine, 5.4 kg of ammonium chloride, 6.8 kg of sodium nitrite, 20 kg of tap water, and Active agent 1.0 kg. The product of the present invention, the consolidated foaming plugging agent, is obtained strictly according to the preparation method described above. As the surfactant, Span-60 was used.
[0050] Indoor medium and low permeability artificial core plugging simulation test comparison: prepared permeability 220×10 -3 μm 2 The artificial cylindrical core has an outer diameter of 25.3mm and a core length of 200.2mm. Use a peristaltic pump to inject the consolidatable foaming plugging agent at a rate of 2mL / min, the injection volume is 0.8PV, and the injection permeability is 215×10 -3 μm 2 artificial core. The breakthrough pressure of the artificial core was tested to be 3.5 MPa after the artificial core was solidified ...
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