Physical method for extracting soybean isoflavone from soybean molasses
A technology of soybean isoflavones and soybean molasses, which is applied in the direction of organic chemistry, can solve the problems of underutilization of soybean isoflavones, complex processes, time-consuming and energy-consuming, etc., and achieve the goals of reducing production costs, simple processes, and improving production efficiency Effect
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Embodiment 1
[0025] The described physical method utilizing soybean molasses to extract soybean isoflavones comprises the following steps:
[0026] (1) sugar adjustment: dilute the soybean molasses with distilled water to be 20% dilute molasses;
[0027] (2) Stirring and extraction: heat dilute molasses to 35°C, and stir and keep warm for 1h;
[0028] (3) Solid-liquid separation: centrifuge the dilute molasses at a speed of 4000rpm for 10 minutes to separate the solid-liquid, remove the clear night in the upper layer, and retain the sediment;
[0029] (4) Ethanol extraction: dissolve the precipitate in an ethanol solution with a volume fraction of 70%, stir for 20 min, and centrifuge to get the supernatant;
[0030] (5) Ethanol recovery: the supernatant in (4) was distilled under negative pressure at a temperature of 55° C. and a vacuum of 0.07 MPa to recover ethanol to obtain creamy soybean isoflavones;
[0031] (6) Re-extraction: re-dissolve the paste soybean isoflavones with an ethano...
Embodiment 2
[0035] The described physical method utilizing soybean molasses to extract soybean isoflavones comprises the following steps:
[0036] (1) sugar adjustment: dilute soybean molasses with distilled water to be 30% dilute molasses;
[0037] (2) Stirring and extraction: heat dilute molasses to 60°C, and stir and keep warm for 1.5h;
[0038] (3) Solid-liquid separation: centrifuge the dilute molasses at a speed of 8000rpm for 25 minutes to separate the solid-liquid, remove the clear night in the upper layer, and retain the sediment;
[0039] (4) Ethanol extraction: dissolve the precipitate in an ethanol solution with a volume fraction of 85%, stir for 40 min, and centrifuge to get the supernatant;
[0040] (5) Ethanol recovery: the supernatant in (4) was distilled under negative pressure at a temperature of 75°C and a vacuum of -0.01MPa to recover ethanol to obtain creamy soybean isoflavones;
[0041] (6) Re-extraction: re-dissolve the paste soybean isoflavones with an ethanol so...
Embodiment 3
[0045] The described physical method utilizing soybean molasses to extract soybean isoflavones comprises the following steps:
[0046] (1) sugar adjustment: dilute soybean molasses with distilled water to be 25% dilute molasses;
[0047] (2) Stirring and extraction: heat dilute molasses to 50°C, and stir and keep warm for 1.2h;
[0048] (3) Solid-liquid separation: centrifuge the dilute molasses at a speed of 5000 rpm for 20 minutes to separate the solid and liquid, remove the clear night in the upper layer, and retain the sediment;
[0049] (4) Ethanol extraction: dissolve the precipitate in an ethanol solution with a volume fraction of 75%, stir for 30 min, and centrifuge to get the supernatant;
[0050] (5) Ethanol recovery: the temperature of the supernatant in (4) is 60° C., and the vacuum degree is 0.03 MPa under negative pressure distillation to recover ethanol to obtain creamy soybean isoflavones;
[0051] (6) Re-extraction: re-dissolve the paste soybean isoflavones ...
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