High-concentration dimethyl tetrachloro dimethylamine brine agent and preparation method thereof
A dimethyltetrachlorodimethylamine salt, high-concentration technology, applied in the fields of botanical equipment and methods, biocides, biocides, etc., can solve the problems of destroying plant living ability, phloem damage, plant death, etc. Spectrum herbicidal effect, strong herbicidal activity, strong systemic effect
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preparation example Construction
[0044] The preparation method of modified tea saponin is as follows:
[0045] (1) Add 15 parts of acrylic acid, 10 parts of methyl acrylate, 10 parts of butyl acrylate and 70 parts of water into a three-necked flask in sequence for stirring at a stirring speed of 100r / min, and a nitrogen flow at a speed of 20ml / min, heated to 45°C under nitrogen atmosphere, and kept for 15 min;
[0046] (2) Add 0.5 parts of polyoxyethylene hydrogenated castor oil and 0.3 parts of sodium lauryl sulfate to step (1), stir evenly, and heat up to 65°C;
[0047] (3) Add 0.2 parts of peroxide initiator to step (2), raise the temperature to 75°C while stirring, and react for 1.5 hours;
[0048] (4) Keep the temperature at 75°C, add 20 parts of tea saponin, and soak for 2 hours.
Embodiment 1
[0051] A kind of preparation method of high-concentration dimethyltetrachlorodimethylamine saline solution comprises the steps: (the mass fraction of dimethyltetrachlorodimethylamine salt in the saline solution is 75%, 2-methyl-4-chloro The specification for phenoxyacetic acid is 96.5%.)
[0052] (1) Ingredients: Weigh 63.52 parts of 2-methyl-4-chlorophenoxyacetic acid, 34.36 parts of dimethylamine and 2.12 parts of modified tea saponin;
[0053] (2) Put 63.52 parts of 2-methyl-4-chlorophenoxyacetic acid and 2.12 parts of modified tea saponin into the preparation kettle in sequence, and adjust the pH value in the preparation kettle to about 4;
[0054] (3) Raise the temperature of the preparation kettle to 55°C, add 34.36 parts of dimethylamine dropwise under agitation at a rate of 10ml / min, after the addition is complete, stir for 30-40min, and monitor in the central control;
[0055] (4) Stand still and filter to produce supernatant and filter residue, test the supernatant,...
Embodiment 2
[0057] A preparation method of high-concentration dimethyltetrachlorodimethylamine saline solution, comprising the steps of: (the mass fraction of dimethyltetrachlorodimethylamine salt in the saline solution is 72.5%, 2-methyl-4-chloro The specification for phenoxyacetic acid is 96.5%.)
[0058] (1) Ingredients: Weigh 61.37 parts of 2-methyl-4-chlorophenoxyacetic acid, 33.20 parts of dimethylamine and 5.43 parts of modified tea saponin;
[0059] (2) Put 61.37 parts of 2-methyl-4-chlorophenoxyacetic acid and 5.43 parts of modified tea saponin into the preparation kettle in sequence, and adjust the pH value in the preparation kettle to about 4;
[0060] (3) Raise the temperature of the preparation kettle to 55°C, add 33.20 parts of dimethylamine dropwise under agitation at a rate of 10ml / min, after the addition is complete, stir for 30-40min, and perform central control testing;
[0061] (4) Stand still and filter to produce supernatant and filter residue, test the supernatant,...
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