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A kind of preparation method of food grade high internal phase emulsion

A high internal phase emulsion, food-grade technology, applied in the field of emulsion preparation, can solve the problems of complicated preparation process of nanoparticles, and achieve the effects of low equipment requirements, simple and feasible process, and low energy consumption.

Active Publication Date: 2022-04-01
QINGDAO AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Aiming at the technical problems encountered in the preparation of food-grade Pickering high internal phase emulsion in the prior art, such as the cumbersome preparation process of nanoparticles and the need for high-speed stirring and emulsification, the present invention provides a preparation method of food-grade high internal phase emulsion

Method used

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  • A kind of preparation method of food grade high internal phase emulsion
  • A kind of preparation method of food grade high internal phase emulsion
  • A kind of preparation method of food grade high internal phase emulsion

Examples

Experimental program
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Effect test

Embodiment 1

[0034] Preparation of 1% ovalbumin solution (w / v): Add 1g ovalbumin into 50mL deionized water, and after fully dissolved, dilute to 100mL with deionized water to obtain 1% ovalbumin solution, store in 4°C refrigerator.

[0035] Preparation of 2% pectin solution (w / v): Add 2 g of pectin into 50 mL of deionized water, stir magnetically until fully dissolved, then dilute to 100 mL with deionized water to obtain 2% pectin solution, store in 4 ℃ refrigerator.

[0036] Mix 15mL of 1% ovalbumin solution and 15mL of 2% pectin solution, adjust the pH of the mixed solution to 3.5, stir and react at 100r / min at room temperature for 10min to form a complex, and then under a constant temperature of 25°C Add soybean oil dropwise while stirring at a speed of 1000r / min until oil flakes are precipitated. At this time, a jelly-like high internal phase emulsion sample A is obtained, and its oil loading (ie internal phase) reaches 80%. . However, the oil loading capacity of 1% ovalbumin and 2%...

Embodiment 2

[0038]Preparation of 2% ovalbumin solution (w / v): Add 2g ovalbumin to 50mL deionized water, then add 0.5844g NaCl, after fully dissolved, dilute to 100mL with deionized water to obtain 2% ovalbumin Protein solution, stored in 4°C refrigerator.

[0039] Preparation of 2% sodium alginate solution (w / v): Add 2g of sodium alginate to 50mL of deionized water, then add 0.5844g of NaCl, after fully dissolved, dilute to 100mL with deionized water to obtain 2% alginic acid Sodium solution, stored in a 4°C refrigerator.

[0040] Mix 15mL of 2% ovalbumin solution with 15mL of 2% sodium alginate solution, adjust the pH of the mixed solution to 4.5, stir and react at 200r / min at room temperature for 15min to form a complex, and then under a constant temperature of 20°C Add V dropwise while stirring at a speed of 900r / min E Oil, until there will be oily flowers precipitated, at this time, a jelly-like high internal phase emulsion sample B with an oil loading capacity of 80.5% is obtained....

Embodiment 3

[0042] Preparation of 1% whey protein isolate solution (w / v): Add 1.0g whey protein isolate into 50mL deionized water, fully dissolve and then dilute to 100mL with deionized water to obtain 1.0% whey protein isolate solution , stored in a 4°C refrigerator.

[0043] Preparation of 2% pectin solution (w / v): Add 2g of pectin into 50mL of deionized water, and after fully dissolved, dilute to 100mL with deionized water to obtain a 2% pectin solution, which is stored in a refrigerator at 4°C.

[0044] Mix 15mL of 1.0% whey protein isolate solution with 15mL of 2.0% pectin solution, adjust the pH of the mixed solution to 3.5, stir and react at 300r / min at room temperature for 10min to form a complex, and then re-form the complex at a constant temperature of 25°C Add walnut oil dropwise while stirring at a rotating speed of 800r / min until some oil flakes are precipitated. At this time, a jelly-like high internal phase emulsion sample C with an oil loading capacity of 76.4% is obtained...

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Abstract

The invention discloses a novel preparation method of a food-grade high internal phase emulsion, which comprises the following steps: (1) mixing a polysaccharide solution and a protein solution, adjusting the pH value, and stirring at a low speed at room temperature until the solution becomes turbid; (2) keeping the temperature while Add the oil dropwise into the solution while stirring, until the oil flower will be precipitated, that is, a high internal phase emulsion will be formed. The raw materials used in the preparation method of the high internal phase emulsion of the present invention are all food-grade, have high safety, mild preparation conditions, simple operation, no need to use emulsifiers and homogeneous emulsification equipment, and are easy to industrialized production. In terms of new food additives and new food development with broadly application foreground.

Description

technical field [0001] The invention belongs to the technical field of emulsion preparation, and in particular relates to a method for preparing a food-grade high internal phase emulsion. Background technique [0002] A high internal phase emulsion refers to an emulsion in which the volume fraction of the dispersed phase (that is, the internal phase) is above 74%, or even as high as 99%. Generally, the volume fraction of the dispersed phase of the emulsion can reach up to 50%, and the droplets in the dispersed phase are dispersed in the continuous phase in the form of unconnected spheres. If the volume fraction of the dispersed phase is increased to more than 74%, that is, a high internal phase emulsion, the dispersed phase droplets will deform into "multifaceted liquid cells" separated by the continuous phase film, and eventually occupy the entire space. Due to the formation of multifaceted liquid cells in the high internal phase emulsion, the system becomes a non-free flo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08J3/03C08J3/07C08L91/00C08L5/06C08L5/04C08L89/00
CPCC08J3/03C08J3/07C08J2489/00C08J2391/00C08J2405/04C08J2405/06
Inventor 黄国清肖军霞朱翠萍
Owner QINGDAO AGRI UNIV