Forging method for high purity niobium ingot used for radio frequency superconducting cavity
A radio frequency superconducting cavity and high-purity technology, applied in the field of forging, can solve the problems of not being able to meet the requirements of mass production and technology promotion of high-purity niobium products, large investment costs for equipment and tooling molds, and long processing cycles for equipment forging dies, etc. , to achieve the effect of being easy to popularize, overcoming the small weight of the billet and short production cycle
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Embodiment 1
[0023] The forging method of the present embodiment comprises the following steps:
[0024] Step 1. Machining the high-purity niobium ingot with a diameter of Φ224mm. After processing, the diameter of the ingot is 212mm. Use a lathe to remove the crust layer formed on the surface after the ingot is smelted and solidified, and remove the surface of the high-purity niobium ingot. In the getter layer, remove the riser and bottom pad with a sawing machine, and measure the chemical composition of the high-purity niobium ingot. The mass content of niobium is 99.99%, and the interstitial impurity element content (wt%): O content is 6.4ppm, The C content is 4.1ppm, the N content is 7ppm, and the H content is 1ppm. The residual resistivity test result of the high-purity niobium ingot is 328;
[0025] Step 2, use a sawing machine to saw and blank the high-purity niobium ingot that removes the riser and the bottom pad in step 1 to obtain a high-purity niobium blank; (Blank height / Blank ...
Embodiment 2
[0033] The forging method of the present embodiment comprises the following steps:
[0034]Step 1. Machining the high-purity niobium ingot with a diameter of Φ217mm. After processing, the diameter of the ingot is 209mm. First, use a lathe to remove the crust layer formed on the surface after the ingot is smelted and solidified, and remove the surface of the high-purity niobium ingot. The getter layer, and then remove the riser and bottom pad with a sawing machine, and measure the chemical composition of the ingot. The mass content of niobium is 99.95%, and the interstitial impurity element content (wt%): O content is 5.4ppm, C The content is 8.1ppm, the N content is 3.9ppm, H≤1ppm, and the ingot residual resistivity test result is 340;
[0035] Step 2, use a sawing machine to saw and blank the high-purity niobium ingot that removes the riser and bottom pad in step 1 to obtain a high-purity niobium billet; the height of the high-purity niobium billet is 415mm, and the height-to...
Embodiment 3
[0043] The forging method of the present embodiment comprises the following steps:
[0044] Step 1. Machining the high-purity niobium ingot with a diameter of Φ219mm. After processing, the diameter of the ingot is 204mm. First, use a lathe to remove the condensate layer formed on the surface after the ingot is smelted and solidified, and remove the surface of the high-purity niobium ingot. The getter layer, and then remove the riser and bottom pad with a sawing machine, and measure the chemical composition of the ingot. The mass content of niobium is 99.99%, and the interstitial impurity element content (wt%): O content is 8.1ppm, C The content is 5.5ppm, the N content is 3.9ppm, H≤1ppm, and the ingot residual resistivity test result is 363;
[0045] Step 2, use a sawing machine to saw and blank the high-purity niobium ingot that removes the riser and the bottom pad in step 1 to obtain a high-purity niobium blank; (blank height / blank diameter) is 2.2;
[0046] Step 3. Carry ...
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