Methods for extracting pterocarpus macrocarpus dye and dyeing fabric
A technology of large fruit red sandalwood and dyes, applied in dyeing methods, natural dyes, azo dyes, etc., can solve problems such as no literature reports, and achieve the effect of elegant fragrance, good color fastness, and avoiding environmental pollution.
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Embodiment 1
[0017] The extraction steps of the red sandalwood dye in this example are as follows: take the waste materials of red sandalwood, etc., dry them in an oven at 60°C for 2 hours, pulverize them to 100 meshes by low-temperature ultra-micro-mechanical, and use the volume percentage concentration of the crushed red sandalwood to Extract with 75% ethanol solution, the mass ratio of solid to liquid is 1:30, adjust PH=8 with plant ash, ultrasonically extract at 60°C for 2 hours, vacuum filter, extract the filter residue again with the same method, and combine the two filtrates , concentrated by vacuum distillation with a rotary evaporator to obtain natural dyes.
[0018] The dyeing process steps of Daguo red sandalwood dye on fabrics such as nylon and wool are as follows:
[0019] (1) preparation of dye liquor: the red sandalwood dye, alum, leveling agent and water prepared in claim 1 are formulated with the following mass percentages, 6 parts of said red sandalwood dye, 3 parts of sa...
Embodiment 2
[0023] The extraction procedure of the dyestuff in this example is as follows: take the waste material of red sandalwood, etc., dry it in an oven at 60°C for 2 hours, pulverize it to 50 mesh by low-temperature ultra-micro-mechanical, and use a volume percentage concentration of 75% of the crushed red sandalwood. The ethanol aqueous solution extraction, the mass ratio of solid to liquid is 1:30, the pH value of the solution is adjusted to about 8 with plant ash, ultrasonic extraction at 60°C for 2 hours, vacuum filtration, the filter residue is extracted again by the same method, and the two filtrates are combined , concentrated by rotary evaporator under reduced pressure distillation to obtain natural red sandalwood dye.
[0024] The dyeing process steps of the large-fruit red sandalwood dye on fabrics such as nylon and wool as claimed in claim 1 are:
[0025] (1) preparation of dye liquor: the red sandalwood dye, alum, leveling agent and water prepared in claim 1 are formulat...
Embodiment 3
[0029] The extraction procedure of the dyestuff in this example is as follows: take the waste material of red sandalwood, etc., dry it in an oven at 70°C for 2 hours, pulverize it to 50 mesh by low-temperature ultra-micro-mechanical, and use PH=7, volume percentage to grind the crushed red sandalwood. The concentration is 75% ethanol plant ash aqueous solution as the extractant, the mass ratio of solid to liquid is 1:40, and the temperature is 60 ° C. After ultrasonic extraction for 2 hours, vacuum filtration, the filter residue is extracted again by the same method, and the two filtrates are combined. Rotary evaporator vacuum distillation, concentration, natural dyes.
[0030] The dyeing process steps of the large-fruit red sandalwood dye on fabrics such as nylon and wool as claimed in claim 1 are:
[0031] (1) preparation of dye liquor: the red sandalwood dye, alum, leveling agent and water prepared in claim 1 are formulated with the following mass percentages, 5 parts of sa...
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