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Method for extracting anthocyanin from fructus aroniamelanocarpae pomace

A kind of technology of Sorbus nigricarpa and anthocyanin, which is applied in the field of plant extraction, can solve the problems of anthocyanin degradation physiological activity, low extraction efficiency, and large concentration volume, so as to shorten the concentration time, reduce energy consumption, increase net effect

Inactive Publication Date: 2017-12-26
黑龙江省尚志绿野浆果有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional solvent extraction methods mostly use hot solvents (40-70°C), add solvent in a large ratio of 1:10-30 times, and extract by leaching for 1-3 hours. This kind of process has low extraction efficiency, large concentration volume, and energy consumption. High, and hot solvents are likely to cause anthocyanin degradation and decrease in physiological activity

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A method for extracting anthocyanins from Aronia arvensis fruit pomace, comprising the steps of:

[0021] (1) The pomace obtained after pulping Aronia berries and separating the juice, mixed with the first extract, adjusting the temperature to 6°C, adding malic acid to make the pH=3.5, stirring and extracting for 4 hours; plate Frame filtration obtains the first filtrate and the first filter residue; the filter cloth of plate and frame filtration is 400 orders; the ratio of the pomace and the first extract is 1kg:4L, and the volume concentration of the first extract is 70%. The aqueous ethanol solution (extraction operation for the first time);

[0022] (2) Mix the first filter residue with the second extract, adjust the temperature to 6°C, add malic acid to make the pH=3.5, stir and extract for 3 hours; plate and frame filter to obtain the second filtrate and the second filter residue; plate and frame filter The filter cloth is 400 mesh; the ratio of the first filter ...

Embodiment 2

[0027] A method for extracting anthocyanins from Aronia arvensis fruit pomace, comprising the steps of:

[0028] (1) The pomace obtained after pulping Aronia berries and separating the juice, mixed with the first extract, adjusting the temperature to 6°C, adding malic acid to make the pH=3.5, stirring and extracting for 4 hours; plate Frame filtration obtains the first filtrate and the first filter residue; the filter cloth of plate and frame filtration is 400 orders; the ratio of the pomace and the first extraction solution is 1kg:5L, and the first extraction solution uses the last batch of The second filtrate plus volume concentration is the required amount of 75% aqueous ethanol to the first extract;

[0029] (2) Mix the first filter residue with the second extract, adjust the temperature to 6°C, add malic acid to make the pH=3.5, stir and extract for 3 hours; plate and frame filter to obtain the second filtrate and the second filter residue; plate and frame filter The fil...

Embodiment 3

[0034] A method for extracting anthocyanins from Aronia arvensis fruit pomace, comprising the steps of:

[0035] (1) The pomace obtained after beating Aronia berries into pulp and separating the juice, mixed with the first extract, adjusting the temperature to 4°C, adding malic acid to make the pH=3, stirring and extracting for 5 hours; plate Frame filtration obtains the first filtrate and the first filter residue; the filter cloth of the plate and frame filtration is 400 orders; the ratio of the pomace and the first extract is 1kg:3L, and the first extract uses the last batch of The second filtrate plus volume concentration is the required amount of 60% aqueous ethanol to the first extract;

[0036] (2) Mix the first filter residue with the second extract, adjust the temperature to 4°C, add malic acid to make pH=3, stir and extract for 2 hours; plate and frame filter to obtain the second filtrate and the second filter residue; plate and frame filter The filter cloth is 400 m...

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Abstract

The invention discloses a method for extracting anthocyanin from fructus aroniamelanocarpae pomace, which includes the following steps: (1) fructus aroniamelanocarpae pomace and first extract are stirred and extracted under 4 DEG C to 10 DEG C and pH is equal to 3 to 4; and by filtration, first filtrate and first filter residue are obtained; (2) the first filter residue is added with second extract, and is stirred and extracted under 4 DEG C to 10 DEG C and pH is equal to 3 to 4; and by filtration, second filtrate and second filter residue are obtained; (3) by using aqueous ethanol solution, the second filter residue is stirred and extracted under 4 DEG C to 10 DEG C and pH is equal to 3 to 4; (4) the first filtrate is concentrated by reducing pressure; and filtration is carried out; (5) the filtrate is loaded onto macroporous resin, aqueous ethanol solution is used for resolution, resolved solution is collected, and after concentration and drying, an anthocyanin extract is obtained. The method is carried out under low temperature, and the degradation and physiological activity decrease of anthocyanin are prevented. Weak acid prevents the partial and complete hydrolysis of acylated anthocyanin as the result of subsequent evaporation and concentration. The use of the filtrates shortens the time of concentration, reduces energy consumption, and saves new solvent, and the yield of anthocyanin is high.

Description

technical field [0001] The invention relates to a method for extracting anthocyanins from Aronia adenocarpus pomace, belonging to the technical field of plant extraction. Background technique [0002] Aroniamelanocarpa is a species of Rosaceae Aronia genus, a deciduous shrub berry. Native to northeastern North America, it is distributed from the Baltic Sea coast to the Pacific coast. Since the introduction of the species in my country, studies on reproduction, cultivation, and regional tests have been completed successively. This tree species is a precious tree species with edible, medicinal, garden and ecological values. The fruit of Aronia nigra has extraordinary health effects. The fruit and its extracts have special curative effects on cardiovascular and cerebrovascular diseases such as heart disease and hypertension, and are widely used in medicine and functional food industries in Europe and America. Anthocyanins, flavonoids (fresh fruit content as high as 0.25%-0.3...

Claims

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Application Information

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IPC IPC(8): C07D311/62
CPCC07D311/62
Inventor 李立平景卓
Owner 黑龙江省尚志绿野浆果有限责任公司
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