Method for sweating and producing wax material for 3D printing
A 3D printing, basic material technology, applied in additive processing, petroleum wax recycling, wax physical processing, etc., can solve the problems of long production cycle, inability to produce wax products, and product yield decline.
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Embodiment 1
[0063] This embodiment includes four parts: (1) hydrogenation, (2) distillation, (3) sweating, (4) preparation and extrusion.
[0064] (1) Hydrogenation
[0065] The wax oil product of the low-temperature F-T synthesis experimental device of China Petrochemical Corporation (n-paraffin content is 95.50wt%; penetration (55℃)>200 (10 -1 mm). From the penetration at 55°C, it can be seen that the raw material contains a large amount of low melting point substances) as the raw material, and in FHJ-2 catalyst (a Ni / Al 2 O 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, the active metal nickel content in terms of oxide is 40%, the catalyst is subjected to conventional reduction treatment before use) under the action of reaction pressure 5.0MPa, reaction temperature 200 ℃, volume space velocity 1.0 h -1 Hydrogenation is carried out under the condition that the volume ratio of hydrogen to liquid is 500:1 to convert the olefins and oxygenate...
Embodiment 2
[0088] This embodiment includes four parts: (1) hydrogenation, (2) distillation, (3) sweating, (4) preparation and extrusion.
[0089] (1) Hydrogenation
[0090] Same as Example 1.
[0091] (2) Distillation
[0092] Same as Example 1.
[0093] (3) Sweating: including (1) preparation, (2) cooling - high temperature and constant temperature - cooling - low temperature and constant temperature crystallization, (3) heating - constant temperature - warming - constant temperature sweating, (4) refining four steps.
[0094] (1) Preparations
[0095] Connect the sealing system of the sweating dish with the pressurized buffer tank and the compressor; install the decompression buffer tank at the lower part of the sweating dish and connect the vacuum pump; connect the sweating dish jacket and the movable coil with the circulation system, and fix the coil in the On the sweating dish; use water as the heating medium; start the heating function of the circulation system to make the circ...
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