Method for sweating and producing wax material for 3D printing

A 3D printing, basic material technology, applied in additive processing, petroleum wax recycling, wax physical processing, etc., can solve the problems of long production cycle, inability to produce wax products, and product yield decline.

Active Publication Date: 2017-12-29
CHINA PETROLEUM & CHEM CORP +1
View PDF16 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the ordinary sweating process produces soap wax and low melting point paraffin wax at 40°C to 60°C, the solid component (wax with a higher melting point) and the liquid component (wax with a lower melting point) in the sweating process are two types of components. They are in two phases of solid and liquid respectively, but it is difficult to completely separate them
In order to make the final product meet the requirements, the method of prolonging the sweating time (reducing the heating rate) and increasing the sweating termination temperature is usually adopted, but this will lead to a long production cycle and a decrease in product yield; tests have shown that the common sweating process produces products with a melting point above 70°C. For wax products, the carbon distribution width and n-alkane content on the wax in the later stage of sweating have nothing to do with the yield, that is, the carbon distribution width on the wax does not decrease with the decrease of yield, and the n-alkane content does not increase with the decrease of yield, so Ordinary sweat separation process is not suitable for the production of wax products with a m

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] This embodiment includes four parts: (1) hydrogenation, (2) distillation, (3) sweating, (4) preparation and extrusion.

[0064] (1) Hydrogenation

[0065] The wax oil product of the low-temperature F-T synthesis experimental device of China Petrochemical Corporation (n-paraffin content is 95.50wt%; penetration (55℃)>200 (10 -1 mm). From the penetration at 55°C, it can be seen that the raw material contains a large amount of low melting point substances) as the raw material, and in FHJ-2 catalyst (a Ni / Al 2 O 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, the active metal nickel content in terms of oxide is 40%, the catalyst is subjected to conventional reduction treatment before use) under the action of reaction pressure 5.0MPa, reaction temperature 200 ℃, volume space velocity 1.0 h -1 Hydrogenation is carried out under the condition that the volume ratio of hydrogen to liquid is 500:1 to convert the olefins and oxygenate...

Embodiment 2

[0088] This embodiment includes four parts: (1) hydrogenation, (2) distillation, (3) sweating, (4) preparation and extrusion.

[0089] (1) Hydrogenation

[0090] Same as Example 1.

[0091] (2) Distillation

[0092] Same as Example 1.

[0093] (3) Sweating: including (1) preparation, (2) cooling - high temperature and constant temperature - cooling - low temperature and constant temperature crystallization, (3) heating - constant temperature - warming - constant temperature sweating, (4) refining four steps.

[0094] (1) Preparations

[0095] Connect the sealing system of the sweating dish with the pressurized buffer tank and the compressor; install the decompression buffer tank at the lower part of the sweating dish and connect the vacuum pump; connect the sweating dish jacket and the movable coil with the circulation system, and fix the coil in the On the sweating dish; use water as the heating medium; start the heating function of the circulation system to make the circ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Melting pointaaaaaaaaaa
Melting rangeaaaaaaaaaa
Softening pointaaaaaaaaaa
Login to view more

Abstract

The invention discloses a method for sweating and producing a wax material for 3D printing. The method comprises the following steps: performing hydro-conversion on an F-T synthetic product; distilling a hydrogenation product to prepare a sweating raw material suitable for a distillation range; and sweating and blending, thereby obtaining the target product. According to the method disclosed by the invention, stable and tiny bubbles are formed in a wax layer in presence of a bubble stabilizer so as to promote rapid discharge of liquid components on the basis of an ordinary sweating process. High temperature and constant temperature stages are increased in the cooling process, and the liquid components are carried out by utilizing airflow through the wax layer in the sweating process, so that a base material which has a melting point of about 70 DEG C and does not contain any low-melting-point component can be produced by the sweating process. The base material is blended and extruded with a toughened resin, a tackifying resin, animal wax and/or vegetable wax, an antioxidant and pigments so as to obtain the wax product for 3D printing. The method disclosed by the invention has the advantages of being low in production equipment investment, simple in production process, low in operating cost, safe, energy-saving, free from solvent pollution and the like.

Description

technical field [0001] The invention belongs to the technical field of special wax production, and in particular relates to a method for producing 3D printing wax materials by sweating. Background technique [0002] Precision casting is a general term for obtaining precise castings with precise modeling methods, among which investment casting is more commonly used, also known as lost wax casting. The products obtained by investment casting are precise and complex, close to the final shape of the parts, and can be used directly without processing or with little processing. very broad. However, the process of investment casting is complicated, mainly including wax pressing, wax trimming, tree forming, dipping, wax melting, casting molten metal and post-processing, among which the wax mold is basically manufactured manually, which takes a long time. [0003] Rapid Prototype (RP) technology is an advanced manufacturing technology produced in the late 1980s. It is the integrati...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C08L91/06C08L53/02C08L57/02C10G73/36C10G73/40C10G73/42B33Y70/00
CPCB33Y70/00C08L91/06C08L2205/025C08L2205/035C10G73/36C10G73/40C10G73/42C08L53/025C08L57/02C08L53/02
Inventor 孙剑锋郭慧兵解利辉毕文卓孙国权张志银
Owner CHINA PETROLEUM & CHEM CORP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products