A method of sweating to produce waxy materials for 3D printing
A 3D printing, basic material technology, applied in additive processing, petroleum wax refining, petroleum wax recycling and other directions, which can solve the problems of long production cycle, inability to produce wax products, and decreased product yield.
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Embodiment 1
[0063] This embodiment includes: (1) hydrogenation, (2) distillation, (3) sweating, (4) blending and silk extrusion.
[0064] (1) Hydrogenation
[0065] The wax oil product (n-paraffin content is 95.50wt%; penetration (55°C) > 200 (10 -1 mm). It can be seen from the needle penetration at 55°C that the raw material contains a large amount of low-melting point substances) as the raw material, in the FHJ-2 catalyst (a Ni / Al 2 o 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, the content of active metal nickel in terms of oxides is 40%, and the catalyst is subjected to conventional reduction treatment before use), under the action of reaction pressure 5.0MPa, reaction temperature 200°C, volume space velocity 1.0 h -1 Hydrogenation is carried out at a volume ratio of 500:1 to hydrogen to convert olefins and oxygenates therein.
[0066] The hydrogenation product has a weight content of n-alkanes of 97.36%. Chromatography-mass spectrome...
Embodiment 2
[0088] This embodiment includes: (1) hydrogenation, (2) distillation, (3) sweating, (4) blending and silk extrusion.
[0089] (1) Hydrogenation
[0090] With embodiment 1.
[0091] (2) Distillation
[0092] With embodiment 1.
[0093] (3) Sweating: Including (1) preparation, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization, (3) heating - constant temperature - heating - constant temperature sweating, (4) refining four steps.
[0094] (1) Preparation
[0095] Connect the sealing system of the sweating dish with the pressurized buffer tank and the compressor; install the decompression buffer tank and connect the vacuum pump at the lower part of the sweating dish; connect the jacket of the sweating dish and the movable coil with the circulation system, and fix the coil in the On the sweating dish; water is used as the heating medium; the heating function of the circulation system is activated to raise the tem...
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