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Textile auxiliary agent applying graphene in after-finishing procedure

A technology of textile auxiliaries and graphene, which is applied in the direction of textiles and papermaking, fiber treatment, flame-retardant fibers, etc., can solve the problems of static electricity, electric shock, and textile auxiliaries not having antistatic effect in textiles, so as to improve antistatic performance, excellent mechanical properties, and the effect of excellent electrical conductivity

Inactive Publication Date: 2017-12-29
JIANGSU NEW REBA TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, although there are many kinds of textile auxiliaries on the market, none of them have antistatic effect, which causes the produced textiles to generate static electricity, especially in dry and windy autumn, it is easier to generate static electricity, and the human body It will produce an "electric shock" effect, and the existing textile auxiliaries need to be improved

Method used

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  • Textile auxiliary agent applying graphene in after-finishing procedure

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preparation example Construction

[0027] As a preference, the present invention also discloses a preparation method of the above-mentioned textile auxiliaries using graphene in the finishing process, the specific steps are as follows:

[0028] (1) Take each raw material according to the above mass percentage;

[0029] (2) Mix dioctyl sodium sulfosuccinate, ethyl formamidothiazole acetate, epichlorohydrin, ethylenediamine, dimethylolpropionic acid, and epichlorohydrin at a temperature of 6500-9500r / m Stir for 4-6h in the state;

[0030] (3) Heating the stirred mixed solution to 55-70° C., then adding graphene, foaming agent, flame retardant, basalt fiber, and water, and performing ultrasonication in an ultrasonic machine to prepare a finished product.

[0031] As a preference, in the step (3), the ultrasonic power of the ultrasonic machine is 800w, and the ultrasonic time is 6-8h.

Embodiment 1

[0033] The invention discloses a preparation method of a textile auxiliary agent using graphene in the post-finishing process, and the specific steps are as follows:

[0034] (1) Take each raw material according to the above mass percentage;

[0035] (2) Add 8% sodium dioctyl sulfosuccinate, 7% ethyl formylaminothiazole acetate, 15% epichlorohydrin, 10% ethylenediamine, 8% dimethylol propionic acid, epoxy chloride Mix 10% propane and stir for 5 hours at 6800r / m;

[0036] (3) Heat the stirred mixed solution to 60°C, then add 13% graphene, 7% dicyandiamide, 5% dicyclopentyl methyl phosphate, 1% basalt fiber, and 14% water, and carry out the process in an ultrasonic machine. Ultrasound, the ultrasonic power of the ultrasonic machine is 800w, and the ultrasonic time is 7h, that is, the finished product is prepared.

Embodiment 2

[0038] The invention discloses a preparation method of a textile auxiliary agent using graphene in the post-finishing process, and the specific steps are as follows:

[0039] (1) Take each raw material according to the above mass percentage;

[0040](2) Add 3% sodium dioctyl sulfosuccinate, 12% ethyl formylaminothiazole acetate, 10% epichlorohydrin, 8% ethylenediamine, 13% dimethylol propionic acid, epoxy chloride Mix 5% propane and stir for 5 hours at 7500r / m;

[0041] (3) Heat the stirred mixed solution to 60°C, then add 3% graphene, 7% dicyandiamide, 15% methyl methyl phosphate, 9% basalt fiber, and 15% water, and carry out the process in an ultrasonic machine. Ultrasound, the ultrasonic power of the ultrasonic machine is 800w, and the ultrasonic time is 7h, that is, the finished product is prepared.

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Abstract

The invention discloses a textile auxiliary agent applying graphene in an after-finishing procedure. The textile auxiliary agent is prepared from the following components in percentage by mass: 3 percent to 13 percent of sodium diethylhexyl sulfosuccinate, 2 percent to 12 percent of ethyl 2-(formylamino)-4-thiazoleacetate, 10 percent to 20 percent of epichlorohydrin, 5 percent to 15 percent of ethylenediamine, 3 percent to 13 percent of dihydromethyl propionic acid, 5 percent to 15 percent of epichlorohydrin, 3 percent to 13 percent of the graphene, 1 percent to 7 percent of a foaming agent, 5 percent to 15 percent of a flame retardant, 1 percent to 9 percent of basalt fiber and 10 percent to 20 percent of water; a preparation method comprises the following steps: mixing the sodium diethylhexyl sulfosuccinate, the ethyl 2-(formylamino)-4-thiazoleacetate, the epichlorohydrin, the ethylenediamine, the dihydromethyl propionic acid and the epichlorohydrin; heating a stirred mixed solution to 55 DEG C to 70 DEG C; then adding the graphene, the foaming agent, the flame retardant, the basalt fibers and the water and carrying out ultrasonic treatment in an ultrasonic machine. The textile auxiliary agent disclosed by the invention has the advantages of good antistatic effect, good flame-retarding effect and the like.

Description

technical field [0001] The invention relates to the technical field of textiles, in particular to a textile auxiliary agent using graphene in the post-finishing process. Background technique [0002] The finishing process is an important process in the process of textile production and processing. Its basic process is four processes, namely, scouring and bleaching process, dyeing process, printing process and finishing process. [0003] In the finishing process of textiles, processors will add textile auxiliaries, among which textile auxiliaries play an indispensable role in improving the product quality and added value of textiles. It can not only endow textiles with various special functions and styles, such as Soft, anti-wrinkle, anti-shrinkage, waterproof, antibacterial, antistatic, flame retardant, etc., can also improve the dyeing and finishing process, play a role in saving energy and reducing processing costs. The role in the industrial chain is crucial. [0004] A...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/11D06M13/256D06M13/402D06M13/332D06M13/207D06M11/74D06M11/79D06M13/292
CPCD06M13/11D06M11/74D06M11/79D06M13/207D06M13/256D06M13/292D06M13/332D06M13/402D06M2200/30
Inventor 储平徐有琦
Owner JIANGSU NEW REBA TECH CO LTD
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