Double-base precious metal DOC catalyst for purifying diesel exhaust and preparation method thereof
A tail gas purification and noble metal technology, applied in the direction of catalyst activation/preparation, physical/chemical process catalysts, chemical instruments and methods, etc., can solve the problems of poor heat resistance of DOC catalysts, low HC conversion efficiency, loss of activity of noble metal catalyst coatings, etc. problems, to achieve the effect of high temperature aging resistance and high catalytic oxidation performance
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Embodiment 1
[0022] Prepare a slurry with a precious metal loading of 60g / ft3, pt:pd=2:1, and a coating loading of 80g / l. The slurry is composed of 70% alumina and 30% cerium-zirconium oxide; Coating carrier specifications are height*diameter*mesh*wall thickness 80mm*90mm / 400cpsi / 4mil;
[0023] 1. Grinding slurry: Weigh 700g of alumina powder and 300g of cerium-zirconium oxide powder, mix the two, add them to 1500g of water, and prepare an initial slurry with a solid content of 40%, put the initial slurry into sand Grind in the mill, detect the particle size of the slurry during the grinding process, and test the particle size of the slurry with a laser particle size analyzer. When the particle size D50 of the slurry is between 3-5 μm, stop the grinding, take out the slurry from the grinding tank, and fully stir the slurry , the solid content of the test slurry is 40%, and it is set aside.
[0024] 2. Add precious metal solution to the slurry:
[0025] Take by weighing 56.998g of the pal...
Embodiment 2
[0032] Prepare and prepare the monoplatinum precious metal catalyst according to the above method, the precious metal load is 60g / ft3, pt:pd=1:0, the coating load is 80g / l slurry, and the slurry is composed of 70% alumina, cerium zirconium The oxide content is 30% slurry; the coating carrier specification is height*diameter*mesh*wall thickness 80mm*90mm / 400cpsi / 4mil;
[0033] 1. Grinding slurry: Weigh 700g of alumina powder and 300g of cerium-zirconium oxide powder, mix the two, add them to 1500g of water, and prepare an initial slurry with a solid content of 40%, put the initial slurry into sand Grind in the mill, detect the particle size of the slurry during the grinding process, and test the particle size of the slurry with a laser particle size analyzer. When the particle size D50 of the slurry is between 3-5 μm, stop the grinding, take out the slurry from the grinding tank, and fully stir the slurry , the solid content of the test slurry is 40%, and it is set aside.
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