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Light-cured single-component waterborne epoxide, waterproof material and preparation method of waterproof material

A water-based epoxy and waterproof material technology, applied in building insulation materials, building components, buildings, etc., can solve the problems of damage, easy sticking, low bonding strength of modified emulsified asphalt, etc., to improve low temperature flexibility, cost Low, fast curing effect

Active Publication Date: 2018-02-02
JIANGSU SINOROAD TRANSPORTATION SCI & TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The main purpose of the present invention is to overcome the defects existing in the existing epoxy-modified asphalt materials, and provide a light-cured single-component water-based epoxy, waterproof material and preparation method thereof to solve the problem of the existing modified emulsified asphalt bonding The problem of low strength and easy sticking to the wheel will cause damage, so it is more suitable for practical use and has industrial utilization value

Method used

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  • Light-cured single-component waterborne epoxide, waterproof material and preparation method of waterproof material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] (1) First weigh 300g of water, 400g of epoxy resin E51, 10g of acrylic acid, 2g of polymerization inhibitor p-benzoquinone, and 30g of diethylaminoethanol into a 1L reactor, heat the reactor to 50°C and stir for 1 hour. Then put 40g of ethylene glycol monobutyl ether and 20g of unsaturated acid anhydride into the reactor and stir for 20min, then cool down the reactor to 20°C, add 10g of water-based photoinitiator Irgacure4265 and stir rapidly for 1h to obtain a photocurable single-component Waterborne epoxy resin;

[0041](2) Heat 500g of 30# asphalt to 185°C, add 10g of SBS modifier, cut in the colloid mill for 1.5h, add 40g of didodecylphenyl ether disulfonate emulsifier and 510g Water is emulsified to prepare emulsified SBS asphalt; then the emulsified asphalt prepared is cooled to room temperature; the emulsified asphalt cooled to room temperature is put into the reactor while stirring and added the SBR latex of 50g and the single prepared by 120g step (1) One-comp...

Embodiment 2

[0043] (1) First weigh 600g of water, 500g of epoxy resin E44, 30g of acrylic acid, 4g of polymerization inhibitor p-benzoquinone, and 50g of diethylaminoethanol into a 1.5L reactor, heat the reactor to 70°C and stir for 1.5 h, then put 60g ethylene glycol monobutyl ether and 30g unsaturated acid anhydride into the reactor and stir for 30min, then cool the reactor to 20°C, add 15g of water-based photoinitiator Darocur 1173 and then stir rapidly for 1.5h to obtain light Curing one-component water-based epoxy resin;

[0044] (2) Heat 600g of 70# asphalt to 175°C, add 30g of SBS modifier, shear in the colloid mill for 1.5h, add 20g of sodium dodecylbenzenesulfonate emulsifier and 630g of water for emulsification, Prepare emulsified SBS asphalt; then cool the prepared emulsified asphalt to room temperature; put the emulsified asphalt cooled to room temperature into the reaction kettle while stirring and add 100g of SBR latex and 100g of the one-component light-cured prepared by st...

Embodiment 3

[0046] (1) First weigh 600g of water, 600g of epoxy resin E51, 50g of acrylic acid, 6g of polymerization inhibitor p-benzoquinone, and 60g of diethylaminoethanol into a 1.5L reactor, heat the reactor to 60°C and stir for 2 hours , and then put 80g of ethylene glycol monobutyl ether and 40g of unsaturated acid anhydride into the reactor and stirred for 40min, then cooled the reactor to 25°C, added 15g of water-based photoinitiator Irgacure4265 and stirred rapidly for 2h to obtain a photocurable single-component 1 part water-based epoxy resin;

[0047] (2) Heat 500g of 50# asphalt to 180°C, add 20g of SBS modifier, cut in the colloid mill for 1.5h, add 30g of sodium dodecylbenzenesulfonate emulsifier and 520g of water for emulsification, Prepare emulsified SBS asphalt; then cool the prepared emulsified asphalt to room temperature; put the emulsified asphalt cooled to room temperature into the reaction kettle while stirring and add 80g of SBR latex and 200g of the one-component l...

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Abstract

The invention discloses a light-cured single-component waterborne epoxide, a waterproof material and a preparation method of the waterproof material. The light-cured single-component waterborne epoxide is prepared from the following components in parts by mass: 40 to 60 parts of epoxy resin, 1 to 5 parts of acrylic acid, 0.2 to 0.6 part of polymerization inhibitor, 3 to 6 parts of diethylaminoethanol, 4 to 8 parts of ethylene glycol monobutyl ether, 2 to 4 parts of unsaturated anhydride, 1 to 2 parts of waterborne light initiator and 30 to 60 parts of water. The light-cured single-component waterborne epoxide adopts self-made modified emulsified asphalt of a light-cured waterborne epoxide system, is different from an existing double-component epoxy curing agent and a latent epoxy curing agent, has the advantages of being good in long-time room-temperature light-shielding storage stability and long in storage time; the room-temperature light-shielding storage can reach 6 months; the waterborne light initiator is added in the light-cured single-component waterborne epoxide; the curing-agent waterborne epoxide is enabled to be quick in curing speed under the action of natural light; the construction is convenient and the construction period is shortened.

Description

technical field [0001] The invention relates to a waterproof material for roads, in particular to a light-cured one-component water-based epoxy, waterproof material and a preparation method thereof. Background technique [0002] Emulsified asphalt is heat-melted asphalt, and through mechanical action, the asphalt is dispersed in the aqueous solution containing emulsifier in the form of fine droplets to form an oil-in-water asphalt emulsion. Emulsified asphalt can be used as penetrating oil, viscous oil, seal oil, slurry seal, etc., and can also be used for cold regeneration of old asphalt pavement materials, dust-proof treatment of gravel pavement and laying temporary pavement. At present, emulsified asphalt is a widely used building material, but it still has many shortcomings, such as too low softening point, poor heat resistance, and short service life. Although SBR and SBS modified emulsified asphalt has improved its performance, has the advantages of saving energy and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G59/17C08L95/00C08L63/10C08L9/08C08L53/02
CPCC08G59/1466C08L95/00C08L2205/035C08L63/10C08L9/08C08L53/02
Inventor 关永胜徐德根陈香陈李峰刘杰黄麒庞一朋藏冬冬
Owner JIANGSU SINOROAD TRANSPORTATION SCI & TECH CO LTD
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