Herbal essence solid perfume based on composite enzymatic hydrolysis technology and preparation method thereof

A technology of solid perfume and compound enzymolysis, which is applied to the formulation of perfume preparations, medical preparations containing active ingredients, and pharmaceutical formulations, etc., can solve the problems of fast release of solid perfume, disappearance of fragrance, and poor fragrance persistence, etc. It is not easy to lose the fragrance, it is easy to carry and use, and the fragrance lasts for a long time.

Inactive Publication Date: 2018-03-16
QINGYUAN CHUQU INTELLIGENT TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional liquid perfume is in a liquid state and is inconvenient to carry around for reapplying, and there are certain defects. Therefore, on the basis of traditional liquid perfume, solid perfume came into being.
[0003] Solid perfume is the essence dissolved or absorbed in the curing agent, which is divided into stick-shaped and granular solid perfume. The product of solid perfume consists of essence, solvent and curing agent. There are certain shortcomings. On the one hand, the aroma of solid perfume is released quickly, and the fragrance persistence is not as elegant and long as that of liquid perfume. On the other hand, the essence components in solid perfume are easy to volatilize during storage, resulting in long-term storage. The problem of disappearing or fading, so there are also areas for improvement

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A method for preparing herbal essence solid perfume based on compound enzymolysis technology, comprising the steps of:

[0026] 1) Mix maltodextrin, gum arabic, sodium methylcellulose and tapioca porous starch in a mass ratio of 15:10:10:8 as the capsule wall material; neroli oil, iris flower oil, lavender Essential oil, jasmine essential oil and peppermint essential oil are mixed according to the mass ratio of 5:4:3:2:1 as the capsule core material;

[0027] Wherein, the cassava porous starch is prepared by the following method: mix cassava starch and PBS buffer solution of pH 6.8 according to the mass volume ratio of 1g: 30mL to obtain starch slurry; The mass-to-volume ratio was mixed, and the enzymolysis was heated at 50°C for 1 hour to inactivate the enzyme, the enzymolysis solution was centrifuged, the precipitate was washed with water, and dried to obtain the cassava porous starch; wherein, the composite enzyme was composed of α-amylase Combined with glucoamylase...

Embodiment 2

[0034] A method for preparing herbal essence solid perfume based on compound enzymolysis technology, comprising the steps of:

[0035] 1) Mix maltodextrin, gum arabic, sodium methylcellulose and tapioca porous starch in a mass ratio of 20:12:11:10 as the capsule wall material; neroli oil, iris flower oil, lavender Essential oil, jasmine essential oil and peppermint essential oil are mixed according to the mass ratio of 6:4:4:2:1 as the capsule core material;

[0036]Wherein, the cassava porous starch is prepared by the following method: mix cassava starch and PBS buffer solution of pH 6.8 according to the mass volume ratio of 1g: 40mL to obtain starch slurry; The mass volume ratio is mixed, and the enzymolysis is heated at 53°C for 2 hours to inactivate the enzyme, the enzymolysis solution is centrifuged, the precipitate is washed with water, and dried to obtain the cassava porous starch; wherein, the composite enzyme is composed of α-amylase It is compounded with glucoamylas...

Embodiment 3

[0043] A method for preparing herbal essence solid perfume based on compound enzymolysis technology, comprising the steps of:

[0044] 1) Mix maltodextrin, gum arabic, sodium methylcellulose and tapioca porous starch in a mass ratio of 25:14:12:10 as the capsule wall material; neroli oil, iris flower oil, lavender Essential oil, jasmine essential oil and peppermint essential oil are mixed according to the mass ratio of 7:5:5:3:2 as the capsule core material;

[0045] Wherein, the cassava porous starch is prepared by the following method: mix cassava starch and PBS buffer solution of pH 6.8 according to the mass volume ratio of 1g:50mL to obtain starch slurry; The mass-volume ratio is mixed, and the enzymolysis is heated at 55°C for 3 hours to inactivate the enzyme, the enzymolysis solution is centrifuged, the precipitate is washed with water, and dried to obtain the cassava porous starch; wherein, the composite enzyme is composed of α-amylase It is compounded with glucoamylas...

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PUM

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Abstract

The invention discloses herbal essence solid perfume based on a composite enzymatic hydrolysis technology and a preparation method thereof. The solid perfume is prepared by the following steps: weighing maltodextrin, Arabic gum, sodium methyl cellulose and cassava porous starch as capsule wall materials; weighing Neroli, Orris oil, lavender essential oil, jasmine essential oil and peppermint essential oil as capsule core materials; adding the capsule wall materials into water and heating the mixture at the temperature of 50-60 DEG C to dissolve the capsule wall materials, so as to obtain a capsule wall solution; adding the capsule core materials into the capsule wall solution, uniformly mixing the mixture, homogenizing the mixture at the pressure of 30-50MPa for 3-6 min, so as to obtain amixed solution; performing spray drying on the mixed solution, so as to obtain an essence microcapsule; uniformly mixing lanolin, jojoba wax, mink oil, squalane and lecithin, so as to obtain a substrate; adding the essence microcapsule into the substrate, so as to obtain the solid perfume. The solid perfume has the characteristics of being convenient in carrying for supplement wearing and lastingin release of fragrance, and avoiding phenomenon that the fragrance disappears or becomes weak during storage.

Description

technical field [0001] The invention belongs to the technical field of cosmetics, and in particular relates to a herbal essence solid perfume based on composite enzymolysis technology and a preparation method thereof. Background technique [0002] Perfume is a liquid with a special fragrance formed by combining various spices to give objects (usually the human body) a lasting and pleasant smell. Traditional liquid perfumes have certain defects because they are in a liquid state and are inconvenient to carry around for reapplying. Therefore, on the basis of traditional liquid perfumes, solid perfumes have emerged as the times require. [0003] Solid perfume is the essence dissolved or absorbed in the curing agent, which is divided into stick-shaped and granular solid perfume. The product of solid perfume consists of essence, solvent and curing agent. There are certain shortcomings. On the one hand, the aroma of solid perfume is released quickly, and the fragrance persistence...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/92A61K8/73A61K8/55A61K8/31A61K8/11A61Q13/00
CPCA61K8/11A61K8/31A61K8/553A61K8/731A61K8/732A61K8/737A61K8/922A61K8/925A61K2800/56A61K2800/805A61Q13/00
Inventor 刘美君
Owner QINGYUAN CHUQU INTELLIGENT TECH CO LTD
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