Transparent ceramic material and preparation method thereof
A technology of transparent ceramics and raw materials, applied in the field of ceramic materials, can solve the problems of poor quality of finished products, short production cycle, low preparation temperature, etc.
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Embodiment 1
[0017] A kind of transparent ceramic material of the present embodiment, comprises the raw material of following weight part: 65 parts of silicon dioxide, 15 parts of aluminum oxide, 0.3 part of ferric oxide, 0.5 part of calcium oxide, 1 part of potassium oxide, 1 part of oxide Lanthanum, 3 parts magnesium oxide, 2 parts lithium oxide, 2 parts phosphorus trioxide, 6 parts calcium nitride.
[0018] The preparation method of the transparent ceramic material of the present embodiment comprises the following steps:
[0019] (1) Get the transparent ceramic raw materials in the above weight parts, mix them uniformly, add a binder and extrude to obtain a semi-finished product;
[0020] (2) Raise the temperature of the extruded semi-finished product to 1500°C, and immediately cool it down to 380°C, and keep it warm for 50 hours;
[0021] (3) Vacuum sinter the semi-finished product after heat preservation for 5 hours, the vacuum sintering temperature is 1600° C., and the transparent c...
Embodiment 2
[0027] A kind of transparent ceramic material of the present embodiment, comprises the raw material of following weight part: 75 parts of silicon dioxide, 20 parts of aluminum oxide, 0.4 part of ferric oxide, 0.8 part of calcium oxide, 1.5 parts of potassium oxide, 2 parts of oxide Lanthanum, 4 parts magnesium oxide, 3 parts lithium oxide, 3 parts phosphorus trioxide, 7 parts calcium nitride.
[0028] The preparation method of the transparent ceramic material of the present embodiment comprises the following steps:
[0029] (1) Get the transparent ceramic raw materials in the above weight parts, mix them uniformly, add a binder and extrude to obtain a semi-finished product;
[0030] (2) Raise the temperature of the extruded semi-finished product to 1600°C, and immediately cool it down to 500°C, and keep it warm for 70 hours;
[0031] (3) Vacuum sinter the semi-finished product after heat preservation for 8 hours, the vacuum sintering temperature is 1700° C., and the transpare...
Embodiment 3
[0037] A kind of transparent ceramic material of the present embodiment, comprises the raw material of following weight part: 80 parts of silicon dioxide, 25 parts of aluminum oxide, 0.5 part of ferric oxide, 1 part of calcium oxide, 2 parts of potassium oxide, 4 parts of oxide Lanthanum, 5 parts of magnesium oxide, 5 parts of lithium oxide, 4 parts of phosphorus trioxide, 8 parts of calcium nitride.
[0038] The preparation method of the transparent ceramic material of the present embodiment comprises the following steps:
[0039] (1) Get the transparent ceramic raw materials in the above weight parts, mix them uniformly, add a binder and extrude to obtain a semi-finished product;
[0040] (2) Raise the temperature of the extruded semi-finished product to 1700°C, and immediately cool it down to 700°C, and keep it warm for 120 hours;
[0041] (3) Vacuum sinter the semi-finished product after heat preservation for 12 hours, the vacuum sintering temperature is 1900° C., and the...
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