A method for detecting reduced glutathione or triglyceride
A glutathione and triglyceride technology, applied in the field of electrochemistry, can solve problems such as complex operations and expensive equipment, and achieve the effects of low cost, convenient and fast detection, and simple operation
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Embodiment 1
[0040] This embodiment provides a method for detecting reduced glutathione, and the schematic diagram of the principle of glutathione determination is shown in figure 1 .
[0041] Prepare a NADPH solution with a concentration of 2-15mM in the HEPES buffer solution, and detect it separately with a blood glucose meter to obtain a linear relationship between the NADPH concentration and the response value of the blood glucose meter, see figure 2 .
[0042] (1) Detection steps of reduced glutathione in buffer solution:
[0043] Solution A: Mix 10 mM NADPH, 40 U / mL glutathione reductase, 20 U / mL glutathione peroxidase, 50 mMATP, 50 U / mL hexokinase, and 10 mM hydrogen peroxide; mix 8 µL of solution A with 2 µL The HEPES buffer solution was mixed and tested with a blood glucose meter, and the result was recorded as P 1 ; Prepare glutathione solution with a concentration range of 0.1mM to 2mM in HEPES buffer solution, mix 8μL solution A with 2μL glutathione solution, let it stand f...
Embodiment 2
[0049] This embodiment provides a method for detecting triglycerides. The principle schematic diagram of triglycerides determination is shown in Figure 6 .
[0050] (1) Detection steps of triglycerides in buffer solution:
[0051] Dissolve triglycerides in a mixture of 6 mg lecithin and 80 μL chloroform, and dilute to different concentrations with tris-hydrochloric acid buffer solution, and mix the obtained triglyceride solution with 50 U / mL lipase, 50 mM Mix ATP and 50U / mL hexokinase mixture, shake the reaction, take 5 μL of the reaction product and 15 μL 33mM ammonium sulfate, 15mM NAD + Mix with 50U / mL glycerol dehydrogenase, let it stand for 20min, and measure the results with a blood glucose meter to obtain the relationship between the triglyceride concentration and the response value of the blood glucose meter, see Figure 7 , The detection range of triglycerides by the blood glucose meter is 0.5-1.5mM, and the detection limit is 0.17mM.
[0052] (2) Detection steps ...
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