Rice chaff bran extract and its preparation method and application
A technology of extract and rice bran, which is applied in the field of medicine, can solve the problems such as reports on the application of rice chaff bran extract that have not yet been retrieved
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Embodiment 1
[0137] 10t of rice bran enters the wet extrusion extruder, the saturated steam is injected into the pressure of 0.7MPa, the diameter of the nozzle hole of the template is 10mm, and the expansion ratio is 1:1.1-1.2 to obtain a microporous granular material (100-110°C, moisture 14%), and then use Dry it with a flat dryer until the moisture content is about 6%, and the temperature is 55°C. Add n-hexane at 55°C for leaching for 2 hours at a weight-to-volume ratio of 1:5, filter, and recover the solvent to obtain 1805 kg of crude rice bran oil. Stir and heat the crude rice bran oil to 70°C, add 150L of hot water at 70°C, let it settle for 2 hours, and collect the upper layer of crude rice bran oil. Stir and heat to 70°C, add 100L of hot water at 70°C, add 3L of 85% phosphoric acid, stir for 25min for degumming, let it settle for 5h, collect the upper layer of degummed oil, heat to 100°C, vacuum dry and dehydrate, cool to 80°C, stir Put in 10°C cold water to lower the temperature i...
Embodiment 2
[0145] 10t of rice chaff enters the wet extrusion extruder, the saturated steam is injected into the pressure 0.6MPa, the template nozzle hole diameter is 10mm, and the expansion ratio is 1:1.1-1.2 to obtain microporous granular materials (100-110°C, moisture 13%), Then dry it with a flat dryer until the moisture content is about 6%, and the temperature is 60°C. Add isopropanol for leaching at 60°C for 2 hours at a weight-to-volume ratio of 1:7, recover the solvent, and obtain 1886 kg of crude rice bran oil. Stir and heat the crude rice bran oil to 70°C, add 150L of hot water at 70°C, let it settle for 2 hours, and collect the upper layer of crude rice bran oil. Stir and heat to 70°C, add 100L of hot water at 70°C, add 3L of 85% phosphoric acid, stir for 30min for degumming, let it settle for 4h, collect the upper layer of degummed oil, heat to 100°C, vacuum dry and dehydrate, cool to 70°C, stir Pass in 10°C cold water to lower the temperature indirectly, lower the temperatur...
Embodiment 3
[0148]10t of rice bran enters the wet extrusion extruder, the saturated steam is injected into the pressure of 0.8MPa, the diameter of the nozzle hole of the template is 10mm, and the expansion ratio is 1:1.1-1.2 to obtain a microporous granular material (100-110°C, moisture 14%), and then use Dry it with a flat-plate dryer until the water content is about 6%, add isopropanol at 60°C for 2 hours at a weight-to-volume ratio of 1:7, and recover the solvent to obtain 1888 kg of crude rice bran oil. Stir and heat the crude rice bran oil to 70°C, add 150L of hot water at 70°C, let it settle for 2 hours, and collect the upper layer of crude rice bran oil. Stir and heat to 70°C, add 100L of hot water at 70°C, add 3L of oxalic acid, stir for 25min for degumming, let it settle for 5h, collect the upper layer of degummed oil, heat to 100°C, vacuum dry and dehydrate, cool to 80°C, stir and pour into 10 Cool the temperature with cold water indirectly to 20-25°C, continue to stir slowly at...
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