Real silk fabric finishing process adopting antistatic finishing agent fixed by sol-gel method
An antistatic finishing agent, sol-gel method technology, applied in fiber treatment, animal fiber, textiles and papermaking, etc., can solve the problems of poor antistatic effect, poor washing resistance, etc., to improve shrinkage, enhance effect, Long-lasting and effective antistatic properties of fabrics
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Embodiment 1
[0018] A silk fabric finishing process using a sol-gel method to fix an antistatic finishing agent, said process comprising the following steps:
[0019] (1) Add methyl orthosilicate, propyltrimethoxysilane and deionized water into the Erlenmeyer flask, and add hydrochloric acid dropwise to make the pH of the solution 1.5, place it in an ice-water bath, and shake vigorously for 12 minutes;
[0020] (2) Dissolve ethoxylauramide, melamine formaldehyde resin and sodium oleate in water, freeze-dry, then add the mixed powder to the sol obtained in step (1), and shake vigorously for 2 minutes in an ice-water bath;
[0021] (3) Mix the silk fabric with the sodium periodate aqueous solution, and react in the dark for 3 hours under normal temperature conditions. After the reaction, add ethylene glycol to neutralize the residual sodium periodate, wash with deionized water repeatedly, and dry naturally ;
[0022] (4) Soak the silk fabric treated in step (3) in phosphate buffer solution ...
Embodiment 2
[0030] A silk fabric finishing process using a sol-gel method to fix an antistatic finishing agent, said process comprising the following steps:
[0031] (1) Add methyl orthosilicate, propyltrimethoxysilane and deionized water into the Erlenmeyer flask, and add hydrochloric acid dropwise to make the pH of the solution 1.8, place it in an ice-water bath, and shake vigorously for 15 minutes;
[0032] (2) Dissolve ethoxylauramide, melamine formaldehyde resin and sodium oleate in water, freeze-dry, then add the mixed powder to the sol obtained in step (1), and shake vigorously for 3 minutes in an ice-water bath;
[0033] (3) Mix the silk fabric with the sodium periodate aqueous solution, and react in the dark for 4 hours under normal temperature conditions. After the reaction, add ethylene glycol to neutralize the residual sodium periodate, wash with deionized water repeatedly, and dry naturally ;
[0034] (4) Soak the silk fabric treated in step (3) in phosphate buffer for 36 ho...
Embodiment 3
[0042] A silk fabric finishing process using a sol-gel method to fix an antistatic finishing agent, said process comprising the following steps:
[0043] (1) Add methyl orthosilicate, propyltrimethoxysilane and deionized water into the Erlenmeyer flask, and add hydrochloric acid dropwise to make the pH of the solution 2.2, place it in an ice-water bath, and shake vigorously for 20 minutes;
[0044] (2) Dissolve ethoxylaurylamide, melamine formaldehyde resin and sodium oleate in water, freeze-dry, then add the mixed powder to the sol obtained in step (1), and shake vigorously for 4 minutes in an ice-water bath;
[0045] (3) Mix the silk fabric with the sodium periodate aqueous solution, and react in the dark for 6 hours under normal temperature conditions. After the reaction, add ethylene glycol to neutralize the residual sodium periodate, wash with deionized water repeatedly, and dry naturally ;
[0046] (4) Soak the silk fabric treated in step (3) in phosphate buffer for 48 ...
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