Preparation method of anti-mite and antibacterial finishing agent for embroidery
A finishing agent and anti-mite technology, used in fiber treatment, textiles and papermaking, etc., can solve the problems of low gloss, poor anti-mite sterilization, poor anti-mold effect, etc., and achieve good gloss and strong anti-mite and sterilization. , the effect of increasing gloss
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Embodiment 1
[0022] Take by weight 100 parts of deionized water, 1.5 parts of castor oil, 1.5 parts of zinc ethyl phenyl dithiocarbamate, 8 parts of sodium dichromate, 3 parts of vinyl acetate resin, 10 parts of silk fibroin, 4 parts of aluminum oxide, 0.1 part of fatty alcohol polyoxyethylene ether, 4 parts of aluminum acetate, 0.5 part of glacial acetic acid and 2 parts of ethylene glycol.
[0023] Put sodium dichromate, aluminum oxide and aluminum acetate into a grinder and grind for 10 minutes, then put them into a reaction kettle equipped with a thermometer, agitator and a heating device, turn on the agitator and start mixing, gradually raise the temperature to 40°C, and the mixing speed is 200r / min , mixed for 120min.
[0024] Add vinyl acetate resin, deionized water and castor oil in sequence, adjust the mixing speed to 400 r / min, mix for 6 hours, raise the temperature to 100°C, add the remaining raw materials, stir for 50 minutes, put them into a sand mill, sand mill for 20 minutes...
Embodiment 2
[0027] Take by weight 100 parts of deionized water, 5.5 parts of castor oil, 5.5 parts of zinc ethyl phenyl dithiocarbamate, 12 parts of sodium dichromate, 7 parts of vinyl acetate resin, 30 parts of silk fibroin, 12 parts of aluminum oxide, 0.5 parts of fatty alcohol polyoxyethylene ether, 8 parts of aluminum acetate, 4.5 parts of glacial acetic acid and 6 parts of ethylene glycol.
[0028] Put sodium dichromate, aluminum oxide and aluminum acetate into a grinder and grind for 20 minutes, then put them into a reaction kettle with a thermometer, a mixer and a heating device, turn on the mixer and start mixing, gradually raise the temperature to 80°C, and the mixing speed is 400r / min , mixed for 160min.
[0029] Add vinyl acetate resin, deionized water and castor oil in turn, adjust the mixing speed to 600 r / min, mix for 10 hours, raise the temperature to 140°C, add the remaining raw materials, stir for 90 minutes, put them into a sand mill, sand mill for 40 minutes, and filter...
Embodiment 3
[0032] Take by weight 100 parts of deionized water, 3.5 parts of castor oil, 3.5 parts of zinc ethyl phenyl dithiocarbamate, 10 parts of sodium dichromate, 5 parts of vinyl acetate resin, 20 parts of silk fibroin, 8 parts of aluminum oxide, 0.3 parts of fatty alcohol polyoxyethylene ether, 6 parts of aluminum acetate, 2.5 parts of glacial acetic acid and 4 parts of ethylene glycol.
[0033] Put sodium dichromate, aluminum oxide and aluminum acetate into a grinder and grind for 15 minutes, then put them into a reaction kettle with a thermometer, a mixer and a heating device, turn on the mixer and start mixing, gradually raise the temperature to 60°C, and the mixing speed is 300r / min , mixed for 140min.
[0034] Add vinyl acetate resin, deionized water and castor oil in turn, adjust the mixing speed to 500 r / min, mix for 8 hours, raise the temperature to 120°C, add the remaining raw materials, stir for 70 minutes, put them into a sand mill, sand mill for 30 minutes, and filter ...
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