Negative-type Photosensitive Resin Composition and Use thereof
A technology of photosensitive resin and resin composition, applied in optics, opto-mechanical equipment, instruments, etc., can solve problems such as hardness and etch resistance non-conformity, decline, etc., achieve excellent transparency, high cross-linking density, reliable Sexually stable effect
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[0028] Synthesis example - polysiloxane compound
[0029] In this synthesis example, polysiloxane compounds A-1 to A-5 were prepared according to the composition formula shown in Table 1 below. Wherein, the preparation method is roughly as follows.
[0030] Get siloxane monomer and propylene glycol monomethyl ether acetate (PGMEA) and stir at room temperature and slowly drop into phosphoric acid aqueous solution 54 grams (0.216 gram H 3 PO 4 dissolved in 54 grams of water), the temperature was raised to 110° C. for a condensation polymerization reaction, and the reaction time was 2 hours. After the reaction is complete, alcohol and water are removed by distillation. Table 1 shows the weight average molecular weight (MW) and polydispersity index (PDI) after synthesis.
[0031] Table 1
[0032]
[0033] TEOS: Tetraethoxysilane (Tetraethyl orthosilicate), C 8 h 20 o 4 Si, CAS No.: 78-10-4
[0034] PTMS: Phenyltrimethoxysilane (Phenyltrimethoxysilane), C 9 h 14 o 3 ...
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