Method for continuous phase transition extraction of Tilapia mossambica skin oil

A tilapia and extraction technology, applied in the production of fat oil/fat and fat production, can solve the problems of large solvent consumption, long pressing time, low extraction rate, etc., and reduce solvent consumption, energy consumption, extraction pressure, etc. and the results of low analytical pressure, completeness and repeatability

Inactive Publication Date: 2018-05-08
SOUTH CHINA AGRI UNIV
View PDF1 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The mechanical pressing method has long pressing time, low oil yield, many impurities, and poor oil quality, and is rarely used now; cooking method, high temperature has a great impact on fat quality, low extraction rate, and high energy consumption; organic solvent method has a long existence time, The efficiency is low, the solvent consumption is large, and it is eas

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Embodiment 1: A kind of method of continuous phase change extraction tilapia skin oil comprises the following steps:

[0019] (1) Dry the selected high-quality tilapia skin after removing impurities at a temperature of 40° C., and control the moisture content at 15% to obtain the tilapia skin raw material.

[0020] (2) Weigh 10kg of the processed tilapia skin raw material, put it into the extraction kettle of the continuous phase change extraction device, and feed 75L of n-butane, under the conditions of extraction temperature 60°C and extraction pressure 0.2Mpa, to The flow rate of 200L / h flows through the extraction kettle, and the continuous extraction lasts for 130min. After the tilapia skin oil is extracted, it flows into the analysis kettle, the analysis temperature is 50°C, and the analysis pressure is 0.1Mpa. It becomes a gas, and then becomes a liquid through compression, flows through the extraction kettle, extracts the material again, and recycles it. The ex...

Embodiment 2

[0022] Embodiment 2: A kind of method of continuous phase change extraction tilapia skin oil comprises the following steps:

[0023] (1) The selected high-quality tilapia skin after removing impurities is dried at a temperature of 45° C., and the moisture content is controlled at 20% to obtain the tilapia skin raw material.

[0024] (2) Weigh 10kg of the treated tilapia skin raw material, put it into the extraction kettle of the continuous phase change extraction device, pass 80L of n-butane, and under the conditions of extraction temperature of 50°C and extraction pressure of 0.6Mpa, The flow rate of 350L / h flows through the extraction kettle, and the continuous extraction lasts for 70min. After the tilapia skin oil is extracted, it flows into the analysis kettle, the analysis temperature is 55°C, and the analysis pressure is 0.1Mpa. It becomes a gas, and then becomes a liquid through compression, flows through the extraction kettle, extracts the material again, and recycles ...

Embodiment 3

[0025] Embodiment 3: A kind of method of continuous phase change extraction tilapia skin oil, comprises the following steps:

[0026] (1) The selected high-quality tilapia skin after removing impurities is dried at a temperature of 40° C., and the moisture content is controlled at 18%, so as to obtain the tilapia skin raw material.

[0027] (2) Weigh 10kg of the treated tilapia skin raw material, put it into the extraction kettle of the continuous phase-change extraction device, pass 70L of butane, and under the conditions of extraction temperature of 50°C and extraction pressure of 0.2Mpa, flow rate The flow rate of 320L / h flows through the extraction kettle, and the continuous extraction lasts for 180min. After the tilapia skin oil is extracted, it flows into the analysis kettle, the analysis temperature is 50°C, and the analysis pressure is 0.1Mpa. The gas is compressed into a liquid and then flows through the extraction kettle to extract the material again for recycling. ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a method for continuous phase transition extraction of Tilapia mossambica skin oil. The continuous phase transition extraction technology is adopted; according to the extractionconditions, an extraction agent is butane, the solid-liquid ratio is 10 g: 30-75 ml, the extraction temperature is 60-100 DEG C, the extraction pressure is 0.1-1 Mpa, the flow rate of the extractionagent is 200-350 L/h, continuous extraction is performed for 130-200 min, the analysis temperature is 50-60 DEG C, and the analysis pressure is 0-0.1 Mpa. The method has the advantages that extractionis efficient, the product has no solvent residue, and the aroma component retention ratio is high; the extraction pressure and the analysis pressure are lower than supercritical values, and meanwhilethe method has the advantages that the conventional solvent extraction volume is large, the batch handling capacity is large, and the production cost is low; the obtain Tilapia mossambica skin oil isorange yellow, strong in aroma, light in fishy smell, and the functional component DHA content can reach 50% or above.

Description

technical field [0001] The invention belongs to the technical field of animal oil extraction, in particular to a method for extracting tilapia skin oil. Background technique [0002] Tilapia has a wide range of food habits, rapid growth, low oxygen resistance, growth temperature of 16-38 ℃, and strong reproduction. The climate in Guangdong is very suitable for large-scale farming of tilapia. Maoming City, Guangdong Province was awarded "China Tilapia The annual output of tilapia is huge, and the production and processing process produces a large number of by-products, most of which are not effectively utilized, which not only wastes resources but also pollutes the environment. By-products of tilapia are used to produce fish oil, which increases the added value of products and generates economic benefits. [0003] Fish oil is a kind of oil extracted from fatty fish. It is rich in omega-3 polyunsaturated fatty acids and has health benefits such as anti-inflammatory and blood ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C11B1/10
CPCC11B1/10
Inventor 曹庸刘飞李敏雄郭斌
Owner SOUTH CHINA AGRI UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap