Method for continuous phase transition extraction of Tilapia mossambica skin oil
A tilapia and extraction technology, applied in the production of fat oil/fat and fat production, can solve the problems of large solvent consumption, long pressing time, low extraction rate, etc., and reduce solvent consumption, energy consumption, extraction pressure, etc. and the results of low analytical pressure, completeness and repeatability
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Embodiment 1
[0018] Embodiment 1: A kind of method of continuous phase change extraction tilapia skin oil comprises the following steps:
[0019] (1) Dry the selected high-quality tilapia skin after removing impurities at a temperature of 40° C., and control the moisture content at 15% to obtain the tilapia skin raw material.
[0020] (2) Weigh 10kg of the processed tilapia skin raw material, put it into the extraction kettle of the continuous phase change extraction device, and feed 75L of n-butane, under the conditions of extraction temperature 60°C and extraction pressure 0.2Mpa, to The flow rate of 200L / h flows through the extraction kettle, and the continuous extraction lasts for 130min. After the tilapia skin oil is extracted, it flows into the analysis kettle, the analysis temperature is 50°C, and the analysis pressure is 0.1Mpa. It becomes a gas, and then becomes a liquid through compression, flows through the extraction kettle, extracts the material again, and recycles it. The ex...
Embodiment 2
[0022] Embodiment 2: A kind of method of continuous phase change extraction tilapia skin oil comprises the following steps:
[0023] (1) The selected high-quality tilapia skin after removing impurities is dried at a temperature of 45° C., and the moisture content is controlled at 20% to obtain the tilapia skin raw material.
[0024] (2) Weigh 10kg of the treated tilapia skin raw material, put it into the extraction kettle of the continuous phase change extraction device, pass 80L of n-butane, and under the conditions of extraction temperature of 50°C and extraction pressure of 0.6Mpa, The flow rate of 350L / h flows through the extraction kettle, and the continuous extraction lasts for 70min. After the tilapia skin oil is extracted, it flows into the analysis kettle, the analysis temperature is 55°C, and the analysis pressure is 0.1Mpa. It becomes a gas, and then becomes a liquid through compression, flows through the extraction kettle, extracts the material again, and recycles ...
Embodiment 3
[0025] Embodiment 3: A kind of method of continuous phase change extraction tilapia skin oil, comprises the following steps:
[0026] (1) The selected high-quality tilapia skin after removing impurities is dried at a temperature of 40° C., and the moisture content is controlled at 18%, so as to obtain the tilapia skin raw material.
[0027] (2) Weigh 10kg of the treated tilapia skin raw material, put it into the extraction kettle of the continuous phase-change extraction device, pass 70L of butane, and under the conditions of extraction temperature of 50°C and extraction pressure of 0.2Mpa, flow rate The flow rate of 320L / h flows through the extraction kettle, and the continuous extraction lasts for 180min. After the tilapia skin oil is extracted, it flows into the analysis kettle, the analysis temperature is 50°C, and the analysis pressure is 0.1Mpa. The gas is compressed into a liquid and then flows through the extraction kettle to extract the material again for recycling. ...
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