Treatment method for wasted lithium ion batteries
A technology of lithium-ion batteries and treatment methods, applied in battery recycling, waste collector recycling, recycling technology, etc., can solve environmental pollution and other problems, and achieve the effect of avoiding secondary pollution
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Embodiment 1
[0040] Common binders in batteries PVDF (polyvinylidene fluoride, Shandong Dongyue Shenzhou New Material Co., Ltd., model DS202), SBR (styrene-butadiene rubber, Difu Industrial (Shanghai) Co., Ltd., model SD3511S), plasticizer CMC (carboxymethyl cellulose, Difu Industrial (Shanghai) Co., Ltd., model DF9013WB) carries out thermogravimetric analysis, and the results are as follows Figure 1~3 shown. figure 1 It is the PVDF thermogravimetric curve that the embodiment of the present invention 1 provides, figure 2 Be the SBR thermogravimetric curve that the embodiment of the present invention 1 provides, image 3It is the CMC thermogravimetric curve that embodiment 1 of the present invention provides.
[0041] pass Figure 1~3 It can be seen from the results that common binders and plasticizers in batteries can be decomposed at 400 °C.
Embodiment 2
[0043] 1) Take a square waste lithium ion battery (model 2065140), the positive electrode material is lithium iron phosphate, the negative electrode is graphite, the separator is PE, and the content of organic components is 20-25 wt%.
[0044] 2) Put the waste lithium-ion battery into the inner cavity of the pyrolysis equipment equipped with an eddy current heating module, and carry out the pyrolysis treatment under an atmospheric pressure high-temperature water molecule atmosphere, and pyrolyze at a temperature of 400°C for 1 hour. During the pyrolysis process, the organic matter in the battery The components decompose into acid gases such as amorphous carbon and carbon dioxide.
[0045] 3) Pass the waste gas obtained by cracking into lime water with a concentration of 0.6 mol / L after cooling to perform absorption treatment to obtain waste gas from which acid gas has been removed.
[0046] 4) Evaluate the cracking and alkaline solution absorption effects of waste batteries. T...
Embodiment 3
[0048] 1) Take the soft-packed waste lithium ion battery (the model is 18220300 lithium iron phosphate waste lithium battery), the positive electrode material is lithium iron phosphate, the negative electrode material is graphite, the diaphragm is PE, and the content of organic components is 25-30wt%.
[0049] 2) Put the waste lithium-ion battery into the inner cavity of the pyrolysis equipment equipped with an eddy current heating module, and carry out the pyrolysis treatment under an atmosphere of high-temperature water molecules at an atmospheric pressure, and pyrolyze at a temperature of 400°C for 0.8h. During the pyrolysis process, the Organic components decompose into amorphous carbon and acid gases such as carbon dioxide.
[0050] 3) Pass the waste gas obtained by cracking into lime water with a concentration of 0.6 mol / L after cooling to perform absorption treatment to obtain waste gas from which acid gas has been removed.
[0051] 4) Evaluate the cracking and alkaline...
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