Temporary plugging agent for temporary plugging diversion for overcoming high stress difference in shale gas fracturing, and preparation method thereof
A temporary plugging agent, high stress technology
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Embodiment 1
[0027] Add 200 grams of distilled water to a 500 ml reaction vessel, turn on the stirring, and then add 28 grams of xanthan gum, 10 grams of sodium polyacrylate, and 8 grams of ammonium polyphosphate (NH 4 ) 12 P 10 O 31 , 22 grams of sodium rosinate and 32 grams of polyethylene glycol 10000, and the reaction system is gradually heated to 80 ℃, continue to stir for 2 hours, until all dissolved, then cooled to 50 ℃, discharge and vacuum dry to obtain the initial product, proceed Sieving to obtain a 20-60 mesh temporary plugging agent. Or the initial product is heated and melted by a screw extruder and extruded, cut and pelletized with a pelletizer, and formed into particles with a particle size of 5-8mm, or processed into a temporary plugging ball of 5-25mm with an injection molding machine. The temporary plugging agent synthesized by this method is suitable for temporary plugging construction of shale gas wells above 120℃.
Embodiment 2
[0029] Add 200 grams of distilled water to a 500 ml reaction flask, turn on the stirring, and then add 12 grams of Sesbania Gum, 15 grams of Xanthan Gum, 12 grams of sodium polyacrylate, 5 grams of ammonium polyphosphate (NH 4 ) 16 P 14 O 43 , 3 grams of ammonium polyphosphate (NH 4 ) 18 P 16 O 49 , 20 grams of sodium rosinate, 20 grams of polyethylene glycol 10000 and 13 grams of polyethylene glycol 20000, and the reaction system is gradually heated to 80°C, and stirring is continued for 2h until all is dissolved, then the temperature is reduced to 50°C, and the discharging proceeds Vacuum drying to obtain the initial product, which is sieved to obtain a 20-60 mesh temporary plugging agent. Or the initial product is heated and melted by a screw extruder and extruded, cut and pelletized with a pelletizer, and formed into particles with a particle size of 5-8mm, or processed into a temporary plugging ball of 5-25mm with an injection molding machine. The temporary plugging agent s...
Embodiment 3
[0031] The temporary plugging agent prepared in Example 2 was added to the fracturing fluid to determine the performance of the temporary plugging agent. The preferred temporary plugging slippery water fracturing fluid formula: 0.1% drag reducer + 0.1% drainage aid + 0.2% clay stabilizer + 5% powder temporary plugging agent. The experiment was carried out at 120°C, and the performance test results of the temporary plugging agent are shown in Table 1.
[0032] Table 1. Performance test results of temporary plugging agent (120℃)
[0033] project
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