Cesium ion removal method based on bentonite-chitosan composite microspheres
A composite microsphere, chitosan technology, applied in chemical instruments and methods, alkali metal compounds, alkali metal oxides/hydroxides, etc., can solve the problem of untargeted removal of pollutants, lengthy removal method steps, solid-liquid Difficulty in separation and other problems, to achieve a wide range of pH, low requirements for adsorption conditions, and environmental friendliness
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Embodiment 1
[0040] A method for removing cesium ions based on bentonite-chitosan composite microspheres includes adding magnetic porous bentonite-chitosan composite microspheres into waste water containing radionuclide cesium ions, and then shaking at a constant temperature.
[0041] The mass of the magnetic porous bentonite-chitosan composite microsphere is 0.1 g, the cesium ion in the waste water is cesium-133, the concentration is 50 mg / L, and the pH range of the waste water is 3.5.
[0042] The temperature of the constant temperature is 24° C., and the oscillation frequency is 120 r / min.
[0043] The oscillating adsorption time is 12h.
[0044] "Adding magnetic porous bentonite chitosan composite microspheres to wastewater containing radionuclide cesium ions, and then shaking at a constant temperature", has excellent adsorption performance for cesium ions, large adsorption capacity, and the maximum equilibrium adsorption capacity is 57.084mg / g ;The requirement for adsorption is low, ...
Embodiment 2
[0046] A method for removing cesium ions based on bentonite-chitosan composite microspheres includes adding magnetic porous bentonite-chitosan composite microspheres into waste water containing radionuclide cesium ions, and then shaking at a constant temperature.
[0047] The mass of the magnetic porous bentonite-chitosan composite microsphere is 0.1 g, the cesium ion in the waste water is cesium-133, the concentration is 100 mg / L, and the pH range of the waste water is 5.
[0048] The temperature of the constant temperature is 25° C., and the oscillation frequency is 120 r / min.
[0049] The vibration adsorption time is 15h.
Embodiment 3
[0051] A method for removing cesium ions based on bentonite-chitosan composite microspheres includes adding magnetic porous bentonite-chitosan composite microspheres into waste water containing radionuclide cesium ions, and then shaking at a constant temperature.
[0052] The mass of the magnetic porous bentonite-chitosan composite microsphere is 0.1 g, the cesium ion in the waste water is cesium-133, the concentration is 150 mg / L, and the pH range of the waste water is 7.
[0053] The temperature of the constant temperature is 26° C., and the oscillation frequency is 120 r / min.
[0054] The vibration adsorption time is 18h.
[0055] The cesium ion is cesium-133.
[0056] The magnetic porous bentonite-chitosan composite microspheres are obtained by dissolving bentonite in acetic acid solution, mechanically stirring and fully mixing, adding chitosan, and then adding Fe 3+ / Fe 2+ Obtain a mixed solution; prepare a mixed solution of sodium citrate and sodium hydroxide; drop th...
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