Preparation method of potassium aspartate crystals
A technology of potassium aspartate and aspartic acid, which is applied in the field of preparation of potassium aspartate crystals, and can solve problems such as large water consumption
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Embodiment 1
[0031] At 20-25°C, add 40ml of pure water to a 2L three-necked reaction flask, turn on the mechanical stirring, add 133.0g of aspartic acid, turn on the heating to an internal temperature of 50-60°C, add 69.0g of potassium carbonate in batches, and wait for the reaction to be clarified Finally, keep stirring at 50-60°C for 1-2 hours, measure the pH value of 5.8-6.0, adjust the pH value to 6.5-6.8 with 1-2% (potassium carbonate weight percentage) of potassium carbonate; cool down to 40-50°C and add medicinal Activated carbon was stirred for 1-2 hours to filter, the filtrate was cooled to 15-25°C, 1130ml of isopropanol was added to the reaction solution, and the internal temperature was kept at -5-20°C to crystallize for 8-12 hours, suction filtered, and the filter cake was placed at 45 °C in a vacuum oven for 9 hours, collected the material, and obtained an off-white amorphous potassium aspartate hemihydrate product with a yield of 96.2%.
Embodiment 2
[0033] At 20-25°C, add 80ml of pure water to a 5L three-necked reaction flask, turn on the mechanical stirring, add 266.2g of aspartic acid, turn on the heating to an internal temperature of 50-60°C, add 138.2g of potassium carbonate in batches, and wait for the reaction to be clarified Finally, keep stirring at 50-60°C for 1-2 hours, measure the pH value of 5.8-6.0, adjust the pH value to 6.5-6.8 with 1-2% (potassium carbonate weight percentage) of potassium carbonate, cool down to 40-50°C and add medicinal Activated carbon was stirred for 1-2 hours to filter, the filtrate was cooled to 15-25°C, 2260 ml of isopropanol was added to the reaction solution, and the internal temperature was kept at -5-20°C to crystallize for 8-12 hours, suction filtered, and the filter cake was placed in After drying in a vacuum oven at 45°C for 9 hours, the materials were collected to obtain an off-white amorphous potassium aspartate hemihydrate product with a yield of 96.5%.
[0034] Perform XRD...
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