A kind of microwave absorbing material and preparation method thereof
A microwave absorbing material and graphene technology, applied in the field of absorbing materials, can solve the problems of impedance mismatch, high conductivity, etc., achieve good absorbing performance, light weight, and solve the effect of impedance mismatch.
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[0036] A kind of preparation method of microwave absorbing material, specifically carries out according to following steps:
[0037] Step 1, adding polyvinyl alcohol to water to obtain a polyvinyl alcohol solution with a mass concentration of 10%;
[0038] Add graphene-cobalt ferrite, multi-walled carbon nanotubes and polyvinylpyrrolidone into water, wherein the mass ratio of graphene-cobalt ferrite to water is 1:71~1:23, the mass ratio of multi-walled carbon nanotubes to water The ratio is 1:71 to 1:69, the mass ratio of polyvinylpyrrolidone to water is 6:335 to 2:115, ultrasonically dispersed to obtain a dispersion;
[0039] Wherein, the graphene-cobalt ferrite is synthesized by a hydrothermal method, specifically according to the following steps:
[0040] Step 1.1, adding graphene and polyvinylpyrrolidone with a mass ratio of 3:1 into deionized water, and ultrasonically dispersing to obtain a graphene dispersion;
[0041] Step 1.2, Co(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3...
Embodiment 1
[0052] A kind of preparation method of microwave absorbing material, specifically carries out according to following steps:
[0053] Step 1, adding polyvinyl alcohol to water to obtain a polyvinyl alcohol solution with a mass concentration of 10%;
[0054] Graphene-cobalt ferrite, multi-walled carbon nanotubes and polyvinylpyrrolidone are added to water, wherein the mass ratio of graphene-cobalt ferrite to water is 1:71, and the mass ratio of multi-walled carbon nanotubes to water is 1: 71. The mass ratio of polyvinylpyrrolidone to water is 6:335, and ultrasonically dispersed to obtain a dispersion liquid;
[0055] Wherein, the graphene-cobalt ferrite is synthesized by a hydrothermal method, specifically according to the following steps:
[0056] Step 1.1, adding graphene and polyvinylpyrrolidone with a mass ratio of 3:1 into deionized water, and ultrasonically dispersing to obtain a graphene dispersion;
[0057] Step 1.2, Co(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O joi...
Embodiment 2
[0064] A kind of preparation method of microwave absorbing material, specifically carries out according to following steps:
[0065] Step 1, adding polyvinyl alcohol to water to obtain a polyvinyl alcohol solution with a mass concentration of 10%;
[0066] Graphene-cobalt ferrite, multi-walled carbon nanotubes and polyvinylpyrrolidone are added to water, wherein the mass ratio of graphene-cobalt ferrite to water is 1:23, and the mass ratio of multi-walled carbon nanotubes to water is 1: 69. The mass ratio of polyvinylpyrrolidone to water is 2:115, and ultrasonically dispersed to obtain a dispersion liquid;
[0067] Wherein, the graphene-cobalt ferrite is synthesized by a hydrothermal method, specifically according to the following steps:
[0068] Step 1.1, adding graphene and polyvinylpyrrolidone with a mass ratio of 3:1 into deionized water, and ultrasonically dispersing to obtain a graphene dispersion;
[0069] Step 1.2, Co(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O joi...
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