Preparation method and application of thermosetting powder coating
A thermosetting powder and coating technology, used in powder coatings, fire-retardant coatings, epoxy resin coatings, etc., can solve the problems of poor weather resistance, easy corrosion, and performance that cannot fully meet the needs of use, and achieve good fire resistance, improved use performance, The effect of good application prospects
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Embodiment 1
[0024] (1) Add 40 parts of water-based acrylic epoxy resin, 25 parts of polylactic acid resin, 10 parts of hydrogenated rosin pentaerythritol ester, 8 parts of N,N-methylenebisacrylamide, and 5 parts of ethylene bisstearamide to the stainless steel reaction In the still, the internal temperature of the stainless steel reaction kettle was raised to 130°C, and the stirring reaction was carried out at the reaction temperature to obtain a high-temperature reactant, the stirring rate was 150 rpm, and the reaction time was 55 minutes;
[0025] (2) Put 6 parts of kaolin into a 10% hydrochloric acid solution and soak for 20 minutes, filter and wash the resulting precipitate with deionized water for 3 times, collect the precipitate and put it into a high-temperature calciner. Calcined at a temperature of 35 minutes, then naturally cooled to room temperature, and then 40 parts of modified auxiliary agents were added to the calcined product. The mixed solution prepared by deionized water...
Embodiment 2
[0032] (1) Add 45 parts of water-based acrylic epoxy resin, 30 parts of polylactic acid resin, 13 parts of hydrogenated rosin pentaerythritol ester, 10 parts of N,N-methylenebisacrylamide, and 7 parts of ethylene bisstearamide to the stainless steel reaction In the still, the internal temperature of the stainless steel reaction kettle was raised to 140°C, and the stirring reaction was carried out at the reaction temperature to obtain a high-temperature reactant, the stirring rate was 200 rpm, and the reaction time was 60 minutes;
[0033] (2) Put 7 parts of kaolin into a 10% hydrochloric acid solution and soak for 25 minutes, filter and wash the resulting precipitate with deionized water 4 times, collect the precipitate and put it into a high-temperature calciner. Calcined at a temperature of 40 minutes, then naturally cooled to room temperature, and then 50 parts of modified auxiliary agents were added to the calcined product. The modified auxiliary agents were made of dodecyl...
Embodiment 3
[0040] (1) Add 50 parts of water-based acrylic epoxy resin, 35 parts of polylactic acid resin, 16 parts of hydrogenated rosin pentaerythritol ester, 12 parts of N,N-methylenebisacrylamide, and 9 parts of ethylene bisstearamide to the stainless steel reaction In the still, the internal temperature of the stainless steel reaction kettle was raised to 150°C, and the stirring reaction was carried out at the reaction temperature to obtain a high-temperature reactant, the stirring rate was 250 rpm, and the reaction time was 65 minutes;
[0041] (2) Put 8 parts of kaolin into a 10% hydrochloric acid solution and soak for 30 minutes, filter and wash the precipitate with deionized water for 5 times, collect the precipitate and put it into a high-temperature calciner. Calcined at a temperature of 45 minutes, then naturally cooled to room temperature, and then 60 parts of modified additives were added to the calcined product. The modified additives were made of dodecyl alcohol ester, dicy...
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