a golf ball-shaped ag/tio 2 Composite porous microsphere and preparation method thereof
A technology of porous microspheres and golf balls, applied in the direction of microsphere preparation, catalyst activation/preparation, microcapsule preparation, etc., can solve the problems of complex process, high cost, and difficult to control shape, and achieve simple process and low cost Effect
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Embodiment 1
[0013] (1) Weigh 60 g of titanium oxalic acid titanium oxalate to dissolve in 1800 ml of deionized water, 0.8 g of silver nitrate is added to 200 ml of deionized water, and the spray dryer is sprayed at 200 ° C to prepare Ag / TiO. 2 Pretty microspheres;
[0014] (2) When the resulting precursor powder obtained by step (1) is heated to 550 ° C from 10 ° C / min, after cooling for 4 h, it is washed three times with water and ethanol, drying at 60 ° C for 2 h, and prepared golf-shaped Ag / TiO 2 Composite porous microspheres.
Embodiment 2
[0016] (1) Weigh 60 g of titanium oxalic acid titanium oxalate dissolve in 1800 ml of deionized water, 1.6 g of silver nitrate is added to 200 ml of deionized water, spray dry by spray dryer at 200 ° C, preparing Ag / TiO 2 Pretty microspheres;
[0017] (2) When the resulting precursor powder obtained by step (1) is heated to 550 ° C from 10 ° C / min, after cooling for 4 h, it is washed three times with water and ethanol, drying at 60 ° C for 2 h, and prepared golf-shaped Ag / TiO 2 Composite porous microspheres.
Embodiment 3
[0019] (2) Weigh 60 g of titanium oxalic acid titanium oxalate dissolved in 1800 ml of deionized water, 0.4 g of silver nitrate was added to 200 ml of deionized water, spray dry by spray dryer at 200 ° C, prepared Ag / TiO 2 Pretty microspheres;
[0020] (2) When the resulting precursor powder obtained by step (1) is heated to 550 ° C from 10 ° C / min, after cooling for 4 h, it is washed three times with water and ethanol, drying at 60 ° C for 2 h, and prepared golf-shaped Ag / TiO 2 Composite porous microspheres.
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